Preparation, single-crystal X-ray diffraction and high-resolution NMR spectroscopic analyses of N-[(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-D,L-ribitol)-5-yl]trimethylammonium iodide.
The synthesis and isolation of 1,4-anhydro-5-deoxy-5-iodo-2,3-O-isopropylidene-D,L-ribitol and N-[(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-D,L-ribitol)-5-yl]trimethylammonium iodide are described. The products were examined by (1)H, (13)C NMR spectroscopy, and N-[(1,4-anhydro-5-deoxy-2,3-O-isopropylidene-D,L-ribitol)-5-yl]trimethylammonium iodide was additionally analyzed by X-ray crystallography.
Dmochowska
Barbara
B
Department of Chemistry, University of Gdańsk, Poland. bdmochow@chemik.chem.univ.gda.pl
Skorupa
Eugenia
E
Pellowska-Januszek
Lucyna
L
Czarkowska
Monika
M
Sikorski
Artur
A
Wiśniewski
Andrzej
A
D003460:Crystallization; D018360:Crystallography, X-Ray; D007454:Iodides / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D008744:Methylamines / Q000737:chemistry; D008958:Models, Molecular; D015394:Molecular Structure; D000644:Quaternary Ammonium Compounds / Q000138:chemical synthesis / Q000737:chemistry*; D012255:Ribitol / Q000737:chemistry; D014961:X-Ray Diffraction
D007454:Iodides; D008744:Methylamines; D000644:Quaternary Ammonium Compounds; D012255:Ribitol; C023336:trimethylamine