[Determination of trace selenium in edible fungi with graphite furnace atomic absorption spectroscopy].
In the present article, samples were digested by a quartz high-pressure digestion pot, reducing the loss of selenium in digestion. The content of selenium in edible fungi was determined by using graphite furnace atomic absorption spectroscopy, and the results showed that when the content of selenium in edible fungi was determined by using 1% Ni(NO3)2 as a matrix modifier, ashing temperature of 500 degreed C, and atomization temperature of 2 500 degrees C, and rectifying background by deuterium light, the recovery was in the range of 92.1%-115.5%, the relative standard deviation of the method was 1.28%, and the limit of detection was 15.8 microg x L(-1). The method was suitable for the determination of trace selenium in edible fungi with the advantages of being simple, rapid, sensitive, stable and accurate etc., and the results were satisfactory.
Tie
Mei
M
Department of Chemistry, East China Normal University, Shanghai 200062, China.
Zhang
Wei
W
Li
Jing
J
Jing
Kui
K
Zang
Shu-liang
SL
Li
Hua-wei
HW
D000363:Agaricales / Q000737:chemistry*; D005504:Food Analysis; D012643:Selenium / Q000032:analysis*; D013054:Spectrophotometry, Atomic / Q000295:instrumentation / Q000379:methods*
D012643:Selenium