A new 17O-isotopic enrichment method for the NMR characterisation of phosphate compounds.
Heating phosphate compounds under (17)O-enriched water vapour is an easy and rapid method to prepare homogeneously enriched and pure samples for the acquisition of (17)O NMR spectra with a good sensitivity.
Flambard
Alexandrine
A
UCCS, Unité de Catalyse et Chimie du Solide, UMR-CNRS 8181, Ecole Nationale Supérieure de Chimie de Lille, Université des Sciences et Technologies de Lille, BP90108, 59655 Villeneuve d'Ascq, France.
Montagne
Lionel
L
Delevoye
Laurent
L
D009682:Magnetic Resonance Spectroscopy / Q000379:methods* / Q000592:standards*; D010103:Oxygen Isotopes; D010710:Phosphates / Q000737:chemistry*; D012015:Reference Standards; D012680:Sensitivity and Specificity; D014867:Water / Q000737:chemistry
D010103:Oxygen Isotopes; D010710:Phosphates; D014867:Water