title: Multi-scale approach continuously relating the microstructure and the macroscopic mechanical properties of plaster pastes during their settings.
abstract: A new multi-scale experimental approach is proposed to continuously relate the microstructure and the macroscopic mechanical properties of plaster pastes during their settings. (1)H NMR relaxometry is used to follow continuously and not destructively, the degree of hydration and the microstructure evolution during the setting and hardening of plaster paste. Transmission of shear and compressional ultrasonic velocities enable the determination of macroscopic mechanical properties of the material during the setting. On the basis of similar behaviors of Young's modulus and NMR-population of confined water as function of the degree of hydration, we conclude that NMR gives a better understanding of the evolution of the microstructure at the origin of a better control of the macroscopic mechanical properties.
authors.affiliation: Laboratoire de Physique de la Matière Condensée, UMR 7643 du CNRS, Ecole Polytechnique, 91128 Palaiseau Cedex, France.
authors.forename: Hamouda
authors.initials: H
authors.lastname: Jaffel
authors.forename: Jean-Pierre
authors.initials: JP
authors.lastname: Korb
authors.forename: Jean-Philippe
authors.initials: JP
authors.lastname: Ndobo-Epoy
authors.forename: Jean-Pierre
authors.initials: JP
authors.lastname: Guicquero
authors.forename: Vincent
authors.initials: V
authors.lastname: Morin