Fatigue behavior of resin composites in aqueous environments.
OBJECTIVE
Interaction between mechanical and chemical fatigue of resin composites was investigated.


METHODS
Fatigue fracture resistance of composites after (1) water immersion and under (2) dry and (3) aqueous conditions was analyzed using a fatigue crack propagation test. The characteristics of fatigue crack propagation were expressed as the correlation between the fatigue crack growth rate (da/dN) and stress intensity factor range (DeltaK) and by the fatigue crack growth threshold (DeltaKth). Following the fatigue test, a fractographic examination was performed by scanning electron microscopy.


RESULTS
Contrary to common perception, fatigue crack propagation was retarded under aqueous conditions but accelerated after water immersion. In addition, fatigue cracks detoured around inorganic macro-fillers, but penetrated organic fillers.


CONCLUSIONS
It was concluded that the inverse effects of water on fatigue resistance of composites are dependent on the experimental conditions. Moreover, inorganic macro-fillers were shown to be functional in retarding fatigue cracks in composites.
Takeshige
F
F
Osaka University Graduate School of Dentistry, Department of Restorative Dentistry and Endodontology, 1-8, Yamadaoka, Suita, Osaka 565-0871, Japan.
Kawakami
Y
Y
Hayashi
M
M
Ebisu
S
S
D003188:Composite Resins / Q000737:chemistry; D003799:Dental Stress Analysis; D019544:Equipment Failure Analysis; D006868:Hydrolysis; D007101:Immersion; D008422:Materials Testing; D008855:Microscopy, Electron, Scanning; D010316:Particle Size; D012822:Silicon Dioxide; D013997:Time Factors; D014867:Water; D015040:Zirconium
D003188:Composite Resins; C083568:Z100 composite resin; D014867:Water; C092420:Clearfil Photo Posterior; C091838:Clearfil Photo Anterior; D012822:Silicon Dioxide; D015040:Zirconium