Comparison of microshear bond strengths of four self-etching bonding systems to enamel using two test methods.
BACKGROUND
Recent advances in enamel and dentine adhesive technology have resulted in the emergence of many new adhesive systems. Self-etching bonding systems do not require a separate etching step and the newest systems are the "all-in-one" systems which combine etching, priming and bonding into a single application. This study reports laboratory enamel microshear bond strengths of a self-etching priming and three all-in-one systems and also evaluates two different microshear bond test methods.


METHODS
One hundred and nineteen enamel specimens were bonded (0.8 mm diameter) with either Clearfil Protect Bond (Kuraray), Xeno III (Dentsply), G Bond (GC) or One-Up Bond F (Tokuyama) using Palfique Estelite resin composite and stored in 37 degrees Celsius water for seven days. The microshear bond test method used either a blade or wire to apply the shear stress. Results were analysed with one-way ANOVA and post hoc (Tukey) multiple comparison analysis.


RESULTS
Clearfil Protect Bond demonstrated higher and more consistent bond strengths than Xeno III, G Bond or One-Up Bond F. The wire method showed much greater reliability in results, with a coefficient of variation half that of the blade method.


CONCLUSIONS
All-in-one adhesives seem to be less reliable than the two-step self-etching priming adhesive when bonding to enamel. Test method can significantly affect results in the microshear bond test method.
Foong
J
J
School of Dental Science, The University of Melbourne, Victoria.
Lee
K
K
Nguyen
C
C
Tang
G
G
Austin
D
D
Ch'ng
C
C
Burrow
M F
MF
Thomas
D L
DL
D000134:Acid Etching, Dental / Q000379:methods*; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003743:Dental Enamel / Q000648:ultrastructure*; D003799:Dental Stress Analysis / Q000295:instrumentation; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D006801:Humans; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D033081:Shear Strength; D013314:Stress, Mechanical; D013696:Temperature; D013997:Time Factors; D014867:Water / Q000737:chemistry
C503075:Clearfil Protect Bond; D003188:Composite Resins; D017220:Dentin-Bonding Agents; C498353:G-Bond; D008689:Methacrylates; C446260:One-Up-Bond F; C487957:Xeno III; C086113:palfique estelite; D014867:Water