Real-time monitoring of microwave-promoted organometallic ligand-substitution reactions using in situ Raman spectroscopy.
An apparatus has been developed for real-time monitoring of organometallic reactions under microwave irradiation using in situ Raman spectroscopy and its application for monitoring ligand substitution reactions of Mo(CO)6 demonstrated.
Barnard
Thomas M
TM
CEM Microwave Technology, 3100 Smith Farm Road, Matthews, NC 28104, USA. mike.barnard@cem.com
Leadbeater
Nicholas E
NE