Post-irradiation hardening of dual-cured and light-cured resin cements through machinable ceramics.
OBJECTIVE
To evaluate the surface hardness (Knoop Hardness Number) of the thin layer in three light-cured and dual-cured resin cements irradiated through or not through 2.0 mm thick machinable ceramics.


METHODS
A piece of adhesive polyethylene tape with a circular hole was positioned on the surface of the ceramic plate to control the cement layer (approximately 50 microm). The cement paste was placed on the ceramic surface within the circle. The ceramic plate with resin cement paste was placed on a clear micro cover glass over a zirconia ceramic block to obtain a flat surface, and the material was polymerized using a visible-light-curing unit. The surface hardness was recorded at a series of time intervals up to 5 days, starting from the end of a light-irradiation period.


RESULTS
The hardness steadily increased with post-irradiation time and tended towards a maximum, usually reached after 1 or 2 days. In all cases, the increase in hardness was relatively rapid over the first 30 minutes and continued at a lower rate thereafter. The dual-cured resin cement for each material showed a significantly higher hardness value than the light-cured resin cement irradiated either through or not through ceramics at all post-irradiation times. The resin cements cured through ceramic for each material were significantly less hard compared with those cured not through ceramics at all post-irradiation times.
Yoshida
Keiichi
K
Division of Applied Prosthodontics, Nagasaki University, Graduate School of Biomedical Sciences, Japan. keiichi@nagasaki-u.ac.jp
Atsuta
Mitsuru
M
D000704:Analysis of Variance; D002516:Ceramics; D006244:Hardness; D008027:Light; D008422:Materials Testing; D044367:Phase Transition; D019279:Resin Cements / Q000737:chemistry / Q000528:radiation effects*; D013674:Technology, Dental / Q000379:methods; D015040:Zirconium
D019279:Resin Cements; D015040:Zirconium; C028541:zirconium oxide