[Determination of scopolamine in the poisoning case by GC/MS].
OBJECTIVE
To separate and determine scopolamine from the food in a poisoning case by GC/MS.


METHODS
The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction.


RESULTS
The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine.


CONCLUSIONS
The method is accurate and reliable.
Chu
Jian-Xin
JX
The Procuratorate of Zhejiang Province, Hangzhou 310012, China.
Xie
Yu
Y
Zhuo
Xiao-Cong
XC
D005517:Foodborne Diseases / Q000209:etiology*; D005554:Forensic Medicine / Q000379:methods*; D008401:Gas Chromatography-Mass Spectrometry / Q000379:methods*; D006212:Hallucinations / Q000139:chemically induced / Q000175:diagnosis; D006801:Humans; D008297:Male; D011605:Psychoses, Substance-Induced / Q000175:diagnosis / Q000209:etiology; D012601:Scopolamine / Q000032:analysis* / Q000737:chemistry / Q000506:poisoning*; D012680:Sensitivity and Specificity; D019657:Solanaceae / Q000737:chemistry; D012997:Solvents / Q000737:chemistry
D012997:Solvents; D012601:Scopolamine