Calibration, uncertainty, and recovery in the chromatographic sciences.
This paper reviews calibration-, uncertainty-, and recovery-related documents from 10 consensus-based organizations. The main points from each treatise are summarized. Also included is a critique of the various approaches, as well as recommendations for a statistically sound protocol that is more compatible with chromatographic data.
Vanatta
L E
LE
Air Liquide--Balazs Analytical Services, Box 650311, MS 301, Dallas, TX 75265, USA. lynn.vanatta@airliquide.com
Coleman
D E
DE
D002138:Calibration; D002845:Chromatography / Q000379:methods*; D015203:Reproducibility of Results; D035501:Uncertainty