title: Bond strengths of all-ceramics: acid vs laser etching.
abstract: Various applications of dental lasers on dental materials have been proposed for surface modifications. This study evaluated whether laser etching could be an alternative to hydrofluoric acid (HF) etching. One hundred and ten lithia-based all-ceramic specimens (Empress 2) (R: 4 mm, h: 4 mm) were prepared and divided into five groups (n = 22/group). The untreated specimens served as the control, while one of the experimental groups was treated with 9.5% HF for 30 seconds. Three remaining test groups were treated with different laser (Er:YAG laser wavelength:2940 nm, OpusDent) power settings: 300 mJ, 600 mJ and 900 mJ. Ten specimens in each group were luted to the other 10 specimens by a dual-curing cement (Variolink II), and shear-bond strength (SBS) tests were performed (Autograph, crosshead speed: 0.5 mm/minute). The results were statistically analyzed (Kruskal Wallis and Mann Whitney-U, alpha = .05). Mean SBS (MPa) were 31.9 +/- 4.0, 41.4 +/- 4.3, 42.8 +/- 6.2, 29.2 +/- 4.5 and 27.4 +/- 3.8 for the control and HF, 300, 600 and 900 mJ groups, respectively. SEM evaluations revealed different surface morphologies depending on the laser parameters. The differences between HF acid and 300 mJ, when compared with the control, 600 and 900 mJ groups, were significant (p < .05). The 300 mJ laser group exhibited the highest shear-bond strength values, indicating that laser etching could also be used for surface treatments.
authors.affiliation: Ege University School of Dentistry, Department of Prosthodontics, Izmir, Turkey. bulent-gokce@yahoo.com
authors.forename: B
authors.initials: B
authors.lastname: Gökçe
authors.forename: B
authors.initials: B
authors.lastname: Ozpinar
authors.forename: M
authors.initials: M
authors.lastname: Dündar
authors.forename: E
authors.initials: E
authors.lastname: Cömlekoglu
authors.forename: B H
authors.initials: BH
authors.lastname: Sen
authors.forename: M A
authors.initials: MA
authors.lastname: Güngör
mesh_terms: D000134:Acid Etching, Dental / Q000379:methods*; D000538:Aluminum Silicates; D001840:Dental Bonding; D045662:Dental Etching; D003776:Dental Porcelain / Q000737:chemistry*; D004871:Erbium; D006801:Humans; D006858:Hydrofluoric Acid / Q000737:chemistry; D007834:Lasers; D018020:Lithium Compounds / Q000737:chemistry; D008422:Materials Testing; D008855:Microscopy, Electron, Scanning; D019279:Resin Cements / Q000737:chemistry; D033081:Shear Strength; D013314:Stress, Mechanical; D013499:Surface Properties; D015019:Yttrium
chemical_list: D000538:Aluminum Silicates; C118557:Empress 2; D018020:Lithium Compounds; D019279:Resin Cements; C493120:lithia disilicate; D003776:Dental Porcelain; C103502:Variolink; D015019:Yttrium; D004871:Erbium; D006858:Hydrofluoric Acid