Influence of saliva contamination on zirconia ceramic bonding.
OBJECTIVE
The purpose of this study was to investigate the influence of saliva contamination and cleaning methods on adhesive bonding to dental zirconia ceramic with a phosphate-monomer-containing luting resin.


METHODS
After saliva immersion, airborne-particle abraded ceramic specimens were cleaned with water rinsing, with isopropanol, with phosphoric acid gel, or with additional airborne-particle abrasion. Airborne-particle abraded specimens without contamination were used as the control group. Chemical analysis of the ceramic surfaces of all groups was done using X-ray photoelectron spectroscopy (XPS). The influence of contamination and cleaning methods on ceramic bond durability was examined by tensile bond strength (TBS) testing after 3 days or 150 days water storage with 37,500 thermal cycles.


RESULTS
After saliva contamination XPS revealed an organic coating which was not removed completely with water rinsing, with isopropanol, or with phosphoric acid. Using TBS testing a strong influence of contamination and cleaning methods on resin bond strength and its durability was found.


CONCLUSIONS
Saliva contamination significantly affected resin bonds to zirconia ceramic and its durability. Airborne-particle abrasion was the most effective cleaning method.
Department of Prosthodontics, Propaedeutics and Dental Materials, Christian-Albrechts University at Kiel, Arnold-Heller-Str. 16, 24105 Kiel, Germany.
B
B
Yang
H C
HC
Lange-Jansen
M
M
Scharnberg
S
S
Wolfart
K
K
Ludwig
R
R
Adelung
M
M
Kern
D019840:2-Propanol; D020906:Air Abrasion, Dental; D003666:Decontamination / Q000379:methods; D001840:Dental Bonding; D003776:Dental Porcelain; D003799:Dental Stress Analysis; D004866:Equipment Contamination; D005260:Female; D006801:Humans; D008855:Microscopy, Electron, Scanning; D010756:Phosphoric Acids; D019279:Resin Cements; D012463:Saliva; D013052:Spectrometry, X-Ray Emission; D013718:Tensile Strength; D014867:Water; D015040:Zirconium
D010756:Phosphoric Acids; D019279:Resin Cements; D014867:Water; D003776:Dental Porcelain; D015040:Zirconium; C030242:phosphoric acid; D019840:2-Propanol; C028541:zirconium oxide