Dynamic ultrasound-assisted extraction of catechins and caffeine in some tea samples.
A novel dynamic ultrasound-assisted extraction (DUAE) device has been constructed for extraction of five catechins and caffeine in solid sample. The accurate, simple, reproducible and sensitive method for the determination of five catechins and caffeine has been developed and validated. A comparison has been made of the efficiencies by employing DUAE and conventionally static ultrasound-assisted extraction (UAE). The proposed method can not only improve extraction efficiency but also decrease time and solvent consumption. The commercial Chinese tea samples, involving green and black teas, are rapidly analyzed by the proposed DUAE method. The linearity, range, selectivity, precision, accuracy, and robustness also showed acceptable values.
Gu
Xungang
X
Department of Chemistry, University of Science & Technology of China, Hefei 230026, China.
Cai
Jibao
J
Zhang
Zhengzhu
Z
Su
Qingde
Q
D002110:Caffeine / Q000032:analysis*; D002392:Catechin / Q000032:analysis*; D002851:Chromatography, High Pressure Liquid; D015203:Reproducibility of Results; D012680:Sensitivity and Specificity; D012997:Solvents / Q000737:chemistry; D013662:Tea / Q000737:chemistry*; D014465:Ultrasonics
D012997:Solvents; D013662:Tea; D002110:Caffeine; D002392:Catechin