title: Gunshot residue testing in suicides: Part I: Analysis by scanning electron microscopy with energy-dispersive X-ray.
abstract: Several different methods can be employed to test for gunshot residue (GSR) on a deceased person's hands, including scanning electron microscopy with energy-dispersive x-ray spectroscopy (SEM-EDX) and inductively coupled plasma-atomic emission spectrometry (ICP-AES). Each of these techniques has been extensively studied, especially on living individuals. The current studies (Part I and Part II) were designed to compare the use and utility of the different GSR testing techniques in a medical examiner setting. In Part I, the hands of deceased persons who died from undisputed suicidal handgun wounds were tested for GSR by SEM-EDX over a 4-year period. A total of 116 cases were studied and analyzed for caliber of weapon, proximity of wound, and results of GSR testing, including spatial deposition upon the hands. It was found that in only 50% of cases with a known self-inflicted gunshot wound was SEM-EDX positive for at least 1 specific particle for GSR. In 18% of the cases there was a discernible pattern (spatial distribution) of the particles on the hand such that the manner in which the weapon was held could be determined. Since only 50% of cases where the person is known to have fired a weapon immediately prior to death were positive for GSR by SEM-EDX, this test should not be relied upon to determine whether a deceased individual has discharged a firearm. Furthermore, in only 18% of cases was a discernible pattern present indicating how the firearm was held. The low sensitivity, along with the low percentage of cases with a discernible pattern, limits the usefulness of GSR test results by SEM-EDX in differentiating self-inflicted from non-self-inflicted wounds.
authors.affiliation: Bexar County Medical Examiner's Office, San Antonio, Texas 78229, USA. kmolina@bexar.org
authors.forename: D Kimberley
authors.initials: DK
authors.lastname: Molina
authors.forename: Michael
authors.initials: M
authors.lastname: Martinez
authors.forename: James
authors.initials: J
authors.lastname: Garcia
authors.forename: Vincent J M
authors.initials: VJ
authors.lastname: DiMaio
mesh_terms: D000965:Antimony / Q000302:isolation & purification; D001464:Barium / Q000302:isolation & purification; D005389:Firearms; D044709:Forensic Ballistics / Q000379:methods*; D006801:Humans; D007854:Lead / Q000302:isolation & purification; D008855:Microscopy, Electron, Scanning; D012867:Skin / Q000737:chemistry; D013405:Suicide; D014948:Wounds, Gunshot / Q000473:pathology*; D014961:X-Ray Diffraction / Q000379:methods*
chemical_list: D001464:Barium; D007854:Lead; D000965:Antimony