Complete assignments of (1)H and (13)C NMR spectroscopic data for two new triterpenoid saponins from Ilex pernyi.
Ilexpernoside A and ilexpernoside B, two new pentacyclic C(4)-nortriterpenoid saponins, were isolated from the leaves of Ilex pernyi Franch. Their chemical structures were determined by MS, NMR spectroscopy and chemical analysis. Complete assignments of the (1)H and (13)C NMR spectroscopic data were achieved by 1D and 2D NMR experiments (HSQC, HMBC, (1)H-(1)H COSY and NOESY).
Xie
Guang-Bo
GB
School of Pharmaceutical Sciences, Peking University Health Science Center, Beijing 100083, People's Republic of China.
Lei
Lian-di
LD
Tu
Peng-Fei
PF
D030017:Ilex / Q000737:chemistry*; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000379:methods; D053978:Pentacyclic Triterpenes / Q000737:chemistry*; D012503:Saponins / Q000737:chemistry*
D053978:Pentacyclic Triterpenes; D012503:Saponins