TiO2 nanosized powders controlling by ultrasound sol-gel reaction.
We studied that anatase-TiO2 powders prepared from sol-gel process of titanium tetra-isopropoxide (TTIP) were developed under ultrasonic irradiation with different frequency of 28, 45 and 100 kHz. The irradiated ultrasound (US) was controlled by using semi-cylindrical reflection plate that was placed onto the vicinity of reaction vessel. The focused US influenced the reduction of particles size and increased the surface area of resultant nanosized TiO2 powders. We also examined photodegradation of rhodamine 640 dye (Rh-640) solution by the resultant TiO2 under UV light exposure. It was observed that low frequency for TiO2 photocatalyst preparation and low calcination temperature were more affected onto the photodegradation of the dye.
Latt
Kyaing Kyaing
KK
Department of Chemistry, Nagaoka University of Technology, 1603-1 Kamitomioka, Nagaoka 940-2188, Japan.
Kobayashi
Takaomi
T
Department of Chemistry, Nagaoka University of Technology, 1603-1 Kamitomioka, Nagaoka 940-2188, Japan. Electronic address: takaomi@nagaokaut.ac.jp.
D002384:Catalysis; D018360:Crystallography, X-Ray; D005782:Gels; D046529:Microscopy, Electron, Transmission; D053758:Nanoparticles / Q000737:chemistry* / Q000528:radiation effects*; D010316:Particle Size; D011208:Powders; D012997:Solvents; D013056:Spectrophotometry, Ultraviolet; D014025:Titanium / Q000737:chemistry* / Q000528:radiation effects*; D014465:Ultrasonics
D005782:Gels; D011208:Powders; D012997:Solvents; C009495:titanium dioxide; D014025:Titanium