Synthesis of new bis-1,2,4-triazole derivatives.
A series of new 1,2/1,3-bis[o-(N-methylidenamino-3-aryl-5-phenyl-4H-1,2,4-triazole-4-yl)phenoxy]ethane/propane derivatives 4 were prepared in good yields by treatment of 4-amino-3-aryl-5-phenyl-4H-1,2,4-triazoles 2 with certain bis-aldehydes 1.Compounds 4 were reduced with NaBH(4) to afford the corresponding 1,2/1,3-bis[o-(N-methylamino-3-aryl-5-phenyl-4H-1,2,4-triazole-4-yl)phenoxy]ethane/propane derivatives 5. All new compounds were characterized by IR, (1)H-NMR, (13)C-NMR and mass spectral data.
Bekircan
Olcay
O
Department of Chemistry, Giresun Faculty of Arts and Sciences, Karadeniz Technical University, 28049, Giresun, Turkey. obekircan@ktu.edu.tr
Bektas
Hakan
H
D000447:Aldehydes / Q000737:chemistry; D000473:Alkanes / Q000737:chemistry; D009682:Magnetic Resonance Spectroscopy; D012545:Schiff Bases / Q000737:chemistry; D017550:Spectroscopy, Fourier Transform Infrared; D014230:Triazoles / Q000138:chemical synthesis* / Q000737:chemistry*
D000447:Aldehydes; D000473:Alkanes; D012545:Schiff Bases; D014230:Triazoles