Analysis of volatile constituents isolated by hydrodistillation and headspace solid-phase microextraction from Adenostyles briquetii Gamisans.
The volatile fraction of the whole plant and separated organs of Adenostyles briquetii Gamisans (syn. Cacalia briquetii; family Asteraceae), an endemic species from Corsica, has been studied by headspace solid-phase microextraction (HS-SPME), GC and GC-MS(EI and CI). A total of 141 components were identified, representing 93% of the entire amount. The volatile fraction was characterised by sesquiterpene hydrocarbons (52.8%) and oxygenated sesquiterpenes (25.9%). The major components were germacrene D (18.5%), zingiberene (12.9%) and beta-oplopenone (10.8%). The influence of HS-SPME parameters on the extraction of family components is reported for the first time.
Paolini
Julien
J
Université de Corse, Equipe Chimie des Produits Naturels, UMR-CNRS 6134, Quartier Grossetti, BP 52, 20250 Corti, France. EADpaolini@univ-corse.fr
Nasica
Elodie
E
Desjobert
Jean-Marie
JM
Muselli
Alain
A
Bernardini
Antoine-François
AF
Costa
Jean
J
D019659:Asteraceae / Q000737:chemistry*; D009822:Oils, Volatile / Q000737:chemistry*; D035261:Plant Components, Aerial / Q000737:chemistry; D010936:Plant Extracts / Q000737:chemistry*; D010938:Plant Oils / Q000737:chemistry; D012717:Sesquiterpenes / Q000032:analysis; D052617:Solid Phase Microextraction / Q000379:methods*
D009822:Oils, Volatile; D010936:Plant Extracts; D010938:Plant Oils; D012717:Sesquiterpenes