Measurement of microstrains across loaded resin-dentin interfaces using microscopic moiré interferometry.
Little is known about the mechanical behavior of resin-dentin interfaces during loading. The presence of relatively compliant hybrid and adhesive layers between stiffer dentin and resin composite should deform more during compressive loading.


OBJECTIVE
The objective of this study was to measure changes in microstrain across bonded dentin interfaces in real time using a recently developed microscope moiré interferometer.


METHODS
This system used a miniature moiré interferometer, using two CCD cameras for simultaneous recording of longitudinal and transverse deformation fields, a piezotransducer for fringe shifting and use of a microscope objective with magnification up to 600 x. Small beams (1 mm x 2 mm x 6 mm) of moist resin-bonded dentin covered with cross-lined diffraction grating replica were placed in a miniature compression tester to allow controlled loading from 2 to 37 N while imaging the interference fringe patterns.


RESULTS
Resin-dentin interfaces created by bonding dentin with Single Bond/Z100, under compressive loading, exhibited comparatively large strains across the adhesive-hybrid interface. When the wrapped phase maps were unwrapped to permit conversion of fringe order to displacements, the 2-D profiles of strain fields revealed non-uniform strains across the adhesive interface. In the adhesive/hybrid layer zone, the negative strain was larger (i.e. -6000 mu epsilon) than that seen in the adjacent resin composite or underlying mineralized dentin. The changes were elastic because they disappeared when the load was removed.


CONCLUSIONS
Microscopic moiré interferometry can be very useful in revealing real-time strain across bonded interfaces under load.
Wood
Judy D
JD
Mechanical Engineering Department, Clemson University, Clemson, SC, USA.
Sobolewski
Paul
P
Thakur
Varun
V
Arola
Dwayne
D
Nazari
Ahmed
A
Tay
Franklin R
FR
Pashley
David H
DH
D017438:Bisphenol A-Glycidyl Methacrylate / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry*; D001840:Dental Bonding; D003804:Dentin / Q000648:ultrastructure*; D017220:Dentin-Bonding Agents / Q000737:chemistry; D004548:Elasticity; D020342:Finite Element Analysis; D006801:Humans; D007091:Image Processing, Computer-Assisted / Q000379:methods; D008422:Materials Testing; D008853:Microscopy / Q000295:instrumentation; D008954:Models, Biological; D015903:Moire Topography / Q000295:instrumentation / Q000379:methods; D011312:Pressure; D012822:Silicon Dioxide / Q000737:chemistry; D013314:Stress, Mechanical; D013499:Surface Properties; D013696:Temperature; D013997:Time Factors; D014867:Water / Q000737:chemistry; D015040:Zirconium / Q000737:chemistry
D003188:Composite Resins; D017220:Dentin-Bonding Agents; C083568:Z100 composite resin; C115612:single bond; D014867:Water; D017438:Bisphenol A-Glycidyl Methacrylate; D012822:Silicon Dioxide; D015040:Zirconium