Adaptation of the Bridgman anvil cell to liquid pressure mediums.
The advantage of Bridgman anvil pressure cells is their wide pressure range and the large number of wires which can be introduced into the pressure chamber. In these pressure cells, soft solid pressure mediums such as steatite are used. We have succeeded in adapting the Bridgman cell to liquid pressure mediums. With this breakthrough, it is now possible to measure in very good hydrostatic pressure conditions up to 7 GPa, which is about twice the pressure attainable in piston-cylinder cells. The pressure gradient in the cell, estimated from the superconducting transition width of lead, is reduced by a factor of 5 in the liquid medium with respect to steatite. By using nonmagnetic materials for the anvils and the clamp and due to the small dimensions of the latter, our device is specially suitable for magnetotransport measurements in dilution fridges. This pressure cell has been developed to measure very fragile and brittle samples such as organic conductors. Resistivity measurements of (TMTTF)(2)BF(4) performed in a solid and a liquid pressure medium demonstrate the necessity of hydrostatic pressure conditions for the study of organic conductors at high pressures.
Rüetschi
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AS
DPMC, University of Geneva, 24 Quai E.-Ansermet, 1211 Genève 4, Switzerland.
Jaccard
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D
D004867:Equipment Design; D019544:Equipment Failure Analysis; D011312:Pressure; D015203:Reproducibility of Results; D012680:Sensitivity and Specificity; D012996:Solutions / Q000737:chemistry*; D013048:Specimen Handling / Q000295:instrumentation*; D014159:Transducers
D012996:Solutions