Exact one-tailed 100p% upper limits for future sample repeatability relative standard deviations obtained in single- and multilaboratory repeatability studies.
Formulas are derived to obtain exact one-tailed 100p% upper limits (kappa(p) and nu(p)) for future sample repeatability relative standard deviations, based on a noncentral t-distribution, for multi- and single-laboratory repeatability studies, respectively, used in the validation of analytical methods.
McClure
Foster D
FD
U.S. FDA, Center for Food Safety and Applied Nutrition, Office of Food Defense, Communication and Emergency Response, Division of Public Health and Biostatistics, Biostatistics Branch, College Park, MD 20740-3835, USA. fdmc5100@yahoo.com
Lee
Jung K
JK
D000465:Algorithms; D002623:Chemistry Techniques, Analytical / Q000592:standards / Q000706:statistics & numerical data*; D015337:Multicenter Studies as Topic; D015203:Reproducibility of Results