title: Spurring radical reactions of organic halides with tin hydride and TTMSS using microreactors.
abstract: Tributyltin hydride-mediated radical reactions of organic halides were successfully carried out in a continuous flow system using a microreactor. The reactions proceeded within a very short period of time, coupled with quickly decomposing radical initiators such as V-65 and V-70. The continuous flow reaction system was applied to gram scale synthesis of a key intermediate for furofuran lignans.
authors.affiliation: Department of Chemistry, Graduate School of Science, Osaka Prefecture University, Sakai, Osaka 599-8531, Japan.
authors.forename: Takahide
authors.initials: T
authors.lastname: Fukuyama
authors.forename: Masahide
authors.initials: M
authors.lastname: Kobayashi
authors.forename: Md Taifur
authors.initials: MT
authors.lastname: Rahman
authors.forename: Naoya
authors.initials: N
authors.lastname: Kamata
authors.forename: Ilhyong
authors.initials: I
authors.lastname: Ryu