Wettability and bonding of self-etching dental adhesives. Influence of the smear layer.
OBJECTIVE
To evaluate dentin wettability and bonding of self-etching and total-etch adhesives on smear layer-covered and smear layer-free dentin.


METHODS
Three self-etching adhesives (Clearfil SE Bond, AdheSE and Xeno III) and one total-etch adhesive (SingleBond) were evaluated. The substrates were mid coronal smear layer-covered and smear layer-free dentin. Dentin wettability by resins was studied from contact angle measurement using sessile drop method and Axisymmetric Drop Shape Analysis (ADSA). Shear-bond strength was evaluated using a push-out technique (ad hoc design). Data were analysed with two-way ANOVA and Tukey's test.


RESULTS
Similar values of dentin wettability were obtained for all adhesives tested regardless the presence of smear layer. Even though, Xeno III and AdheSE exhibited slightly lower wettability (higher contact angles values) on smear layer-free dentin. Likewise, the presence of smear layer did not affect the shear-bond strength. Total-etch adhesive obtained higher shear-bond strength than self-etching adhesives, which obtained similar values.


CONCLUSIONS
Wettability is similar between self-etching and total-etch adhesives. The smear layer affects slightly the wettability of self-etching adhesives. Shear-bond strength is not sensitive to the smear layer presence. Total-etch adhesion is stronger than self-etching adhesion. There is no clear relationship between wettability and bond strength.
Aguilar-Mendoza
Jose A
JA
Biocolloid and Fluid Physics Group, Department of Applied Physics, University of Granada, Spain.
Rosales-Leal
Juan I
JI
Rodríguez-Valverde
Miguel A
MA
González-López
Santiago
S
Cabrerizo-Vílchez
Miguel A
MA
D000134:Acid Etching, Dental / Q000379:methods; D000180:Acrylic Resins / Q000737:chemistry; D017438:Bisphenol A-Glycidyl Methacrylate / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003804:Dentin / Q000648:ultrastructure*; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D006801:Humans; D008422:Materials Testing; D019279:Resin Cements / Q000737:chemistry; D033081:Shear Strength; D016369:Smear Layer; D013314:Stress, Mechanical; D017155:Wettability
D000180:Acrylic Resins; C489662:AdheSE cement; C438313:Clearfil SE Bond; D003188:Composite Resins; D017220:Dentin-Bonding Agents; D019279:Resin Cements; C487957:Xeno III; C115612:single bond; D017438:Bisphenol A-Glycidyl Methacrylate