title: Effect of aging on the shear bond strength of orthodontic brackets.
abstract: BACKGROUND
  Bracket loss during the later stages of orthodontic treatment is a relatively frequent occurrence. The purpose of this study was to evaluate and isolate the effect of composite aging, one of many factors that can contribute to decreased bond strength during a normal 24-month orthodontic treatment period.
  
  
  METHODS
  Two orthodontic bonding adhesives--Transbond APC II (3M Unitek, Monrovia, Calif) and Quick Cure adhesive (Reliance Orthodontic Products, Itasca, Ill)--were used to bond brackets to 280 bovine incisors that were stored in distilled water at 37 degrees C for 30 minutes, 24 hours, and 1, 6, 12, 18, and 24 months before shear-peel testing.
  
  
  RESULTS
  Bond strength increased over the first 24 hours and then tended to decrease over the next 24 months. The bond strengths (in MPa) for Transbond and Quick Cure, respectively, were as follows: 30 minutes, 14.99 +/- 0.75 and 21.02 +/- 1.79; 24 hours, 20.99 +/- 2.11 and 25.61 +/- 1.96; 1 month, 20.54 +/- 1.58 and 18.96 +/- 1.02; 6 months, 17.77 +/- 1.66 and 19.52 +/- 1.61; 12 months, 14.79 +/- 1.30 and 18.28 +/- 1.43; 18 months, 16.08 +/- 1.37 and 16.19 +/- 1.01; and 24 months, 12.44 +/- 1.06 and 8.62 +/- 1.03.
  
  
  CONCLUSIONS
  Shear bond strength of orthodontic brackets increases from 30 minutes to 24 hours and then tends to decrease over the next 24 months. The decrease in bond strength due to the effects of composite aging in water appears to be a major factor in the decreased bond strength seen clinically.
authors.affiliation: Department of Orthodontics, University of Colorado at Denver and Health Sciences Center, Aurora, CO 80045, USA. larry.oesterle@uchsc.edu
authors.forename: Larry J
authors.initials: LJ
authors.lastname: Oesterle
authors.forename: W Craig
authors.initials: WC
authors.lastname: Shellhart
mesh_terms: D000704:Analysis of Variance; D000818:Animals; D017438:Bisphenol A-Glycidyl Methacrylate; D002417:Cattle; D001840:Dental Bonding; D003799:Dental Stress Analysis; D006868:Hydrolysis; D016910:Orthodontic Brackets; D019279:Resin Cements; D033081:Shear Strength; D013997:Time Factors
chemical_list: C429624:Quick Cure resin cement; D019279:Resin Cements; C065742:Transbond; D017438:Bisphenol A-Glycidyl Methacrylate