Noncontact analysis of the fiber weight per unit area in prepreg by near-infrared spectroscopy.
The fiber weight per unit area in prepreg is an important factor to ensure the quality of the composite products. Near-infrared spectroscopy (NIRS) technology together with a noncontact reflectance sources has been applied for quality analysis of the fiber weight per unit area. The range of the unit area fiber weight was 13.39-14.14mgcm(-2). The regression method was employed by partial least squares (PLS) and principal components regression (PCR). The calibration model was developed by 55 samples to determine the fiber weight per unit area in prepreg. The determination coefficient (R(2)), root mean square error of calibration (RMSEC) and root mean square error of prediction (RMSEP) were 0.82, 0.092, 0.099, respectively. The predicted values of the fiber weight per unit area in prepreg measured by NIRS technology were comparable to the values obtained by the reference method. For this technology, the noncontact reflectance sources focused directly on the sample with neither previous treatment nor manipulation. The results of the paired t-test revealed that there was no significant difference between the NIR method and the reference method. Besides, the prepreg could be analyzed one time within 20s without sample destruction.
Jiang
B
B
Polymer Materials and Engineering Division, Department of Applied Chemistry, Harbin Institute of Technology, P.O. Box: 410, Harbin 150001, People's Republic of China. jiangbo_5981@yahoo.com.cn
Huang
Y D
YD
D002138:Calibration; D002244:Carbon / Q000032:analysis*; D000077482:Carbon Fiber; D008970:Molecular Weight; D012044:Regression Analysis; D015203:Reproducibility of Results; D019265:Spectroscopy, Near-Infrared / Q000295:instrumentation* / Q000379:methods*; D013997:Time Factors
D000077482:Carbon Fiber; D002244:Carbon