Bond strength of luting materials to ceramic crowns after different surface treatments.
The aim of present study was to evaluate the effect of different pre-treatments of alumina and zirconia copings on the bond strength of different luting materials. Pull out tests was performed on 60 alumina and 80 zirconia copings. Randomly selected, copings were divided in groups of i) un-treated alumina and zirconia copings, (n=20) ii) alumina and zirconia copings sandblasted with 50 or 110 microm alumina particles respectively (n=20), iii) zirconia copings treated with monolayer of glass pearls fused to the inner surface (n=20), iv) zirconia copings treated with silanized glass pearls (n=10). Zinc phosphate, Panavia 21 and VarioLink II were used for cementation. Pull out tests were done in an Instron universal testing machine with a speed of 0.5 mm/min and fracture loads was measured in N. Untreated zirconia copings cemented with zinc phosphate showed significantly higher bond strength values compared to those with sandblasted surfaces. No difference was seen between untreated alumina copings and those with sandblasted surfaces. Sandblasting decreased bond strength of zirconia and alumina copings. Glass pearls increased bond strength of zirconia copings, which was even better after silanization. Variolink II in combination with alumina gave significantly lower bond strength.
Derand
T
T
Dental Technology and Dental Materials Science, Faculty of Odontology, Malmö University, Malmö, Sweden. Tore.Derand@od.mah.se
Molin
M
M
Kleven
E
E
Haag
P
P
Karlsson
S
S
D000537:Aluminum Oxide / Q000737:chemistry; D002484:Cementation; D003442:Crowns; D001840:Dental Bonding; D003738:Dental Cements / Q000737:chemistry*; D045662:Dental Etching / Q000379:methods; D003776:Dental Porcelain / Q000737:chemistry*; D017267:Dental Prosthesis Design; D003799:Dental Stress Analysis / Q000295:instrumentation; D005898:Glass / Q000737:chemistry; D006801:Humans; D008422:Materials Testing; D010710:Phosphates / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry; D012821:Silanes / Q000737:chemistry; D013314:Stress, Mechanical; D013499:Surface Properties; D015036:Zinc Phosphate Cement / Q000737:chemistry; D015040:Zirconium / Q000737:chemistry
D003738:Dental Cements; C093719:Panavia TPN-S; D010710:Phosphates; D019279:Resin Cements; D012821:Silanes; D003776:Dental Porcelain; C103502:Variolink; D015036:Zinc Phosphate Cement; D015040:Zirconium; D000537:Aluminum Oxide; C028541:zirconium oxide