Determination of carbon monoxide in tuna by gas chromatography with micro-thermal conductivity detector.
The suitability of a portable gas chromatograph equipped with a micro-thermal conductivity detector for the head-space determination of carbon monoxide (CO) in tuna samples is evaluated; CO is estimated after its liberation from tissue by acidic treatment at 70 degrees C. Using the tested technique, the CO contents in untreated and suspected treated samples are analyzed. A limit of detection of approximately 13 ng/g is reached. The results demonstrate that this apparatus has performances similar to more expensive and sophisticated instruments.
Bernardi
Cristian
C
Department of Veterinary Sciences and Technologies for Food Safety, University of Milan - Via Celoria 10 - 20133 Milan, Italy.
Chiesa
Luca Maria
LM
Soncin
Silvia
S
Passerò
Elena
E
Biondi
Pier Antonio
PA
D002138:Calibration; D002248:Carbon Monoxide / Q000032:analysis*; D002849:Chromatography, Gas / Q000379:methods*; D005396:Fish Products / Q000032:analysis*; D015203:Reproducibility of Results; D012680:Sensitivity and Specificity; D013696:Temperature
D002248:Carbon Monoxide