Growth and characterization of sodium pentaborate [Na(H4B5O10)] single crystals.
The bulk single crystals of sodium pentaborate [Na(H4B5O10)] were grown by slow evaporation solution growth technique using deionized water as solvent. The grown crystal was confirmed by single crystal X-ray diffraction studies. The structural perfection of the grown crystals has been analyzed by high resolution X-ray diffraction (HRXRD) studies by recording rocking curve. The photoluminescence (PL), UV-vis spectral studies were performed and the optical bandgap of the material was calculated. The presence of the functional groups was identified by FT-IR measurement. The factor group analysis was done on Na(H4B5O10) to reveal the vibrational optical modes. The thermal and mechanical properties of the grown crystal were studied by TG-DTA and Vickers microhardness tester, respectively. The dielectric behavior of Na(H4B5O10) was investigated with different frequencies and temperatures.
Stella Mary
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Department of Physics, Anna University, Sardar Patil Road, Guindy, Chennai 600025, India.
Shahil Kirupavathy
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Mythili
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Gopalakrishnan
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D001881:Borates / Q000737:chemistry*; D003460:Crystallization; D004578:Electron Spin Resonance Spectroscopy / Q000379:methods*; D006244:Hardness; D006860:Hydrogen Bonding; D008027:Light; D049449:Luminescence; D010100:Oxygen / Q000737:chemistry; D012964:Sodium / Q000737:chemistry*; D012995:Solubility; D013056:Spectrophotometry, Ultraviolet / Q000379:methods; D017550:Spectroscopy, Fourier Transform Infrared / Q000379:methods; D013314:Stress, Mechanical; D013696:Temperature; D014961:X-Ray Diffraction
D001881:Borates; D012964:Sodium; D010100:Oxygen; C538809:sodium pentaborate