title: [Synthesis and application of novel dental adhesive materials of 10-methacryloyloxydecyl dihydrogen phosphate].
abstract: 10-methacryloyloxydecyl dihydrogen phosphate was synthesized from the reaction of phosphoryl chloride with methylacrylic acid and 1, 10-decanediol. The structure of product was characterized by 1H-NMR, 31P-NMR and MS. The effect of this product on the bond durability of composite resin joined to enamel, dentin and dental alloy was evaluated by the test of shear strengths. 10-methacryloyloxydecyl dihydrogen phosphate significantly elevated the bond strength of the composite resin joined to enamel, dentin, Ti alloy and Co-Cr alloy; the relevant shear strengths were 13.5, 11.2, 16.2 and 18.1 MPa, respectively.
authors.affiliation: Electromechanics and Materials Engineering College, Dalian Maritime University, Dalian 116026, China. lliu@newmail.dlmu.edu.cn
authors.forename: Lian
authors.initials: L
authors.lastname: Liu
authors.forename: Hui
authors.initials: H
authors.lastname: Liu
authors.forename: Xin
authors.initials: X
authors.lastname: Li
authors.forename: Chunqing
authors.initials: C
authors.lastname: Zhang
mesh_terms: D001840:Dental Bonding; D017220:Dentin-Bonding Agents / Q000138:chemical synthesis* / Q000737:chemistry; D006801:Humans; D008689:Methacrylates / Q000138:chemical synthesis* / Q000737:chemistry; D033081:Shear Strength
chemical_list: D017220:Dentin-Bonding Agents; D008689:Methacrylates; C069749:methacryloyloxydecyl dihydrogen phosphate