[Synthesis and application of novel dental adhesive materials of 10-methacryloyloxydecyl dihydrogen phosphate].
10-methacryloyloxydecyl dihydrogen phosphate was synthesized from the reaction of phosphoryl chloride with methylacrylic acid and 1, 10-decanediol. The structure of product was characterized by 1H-NMR, 31P-NMR and MS. The effect of this product on the bond durability of composite resin joined to enamel, dentin and dental alloy was evaluated by the test of shear strengths. 10-methacryloyloxydecyl dihydrogen phosphate significantly elevated the bond strength of the composite resin joined to enamel, dentin, Ti alloy and Co-Cr alloy; the relevant shear strengths were 13.5, 11.2, 16.2 and 18.1 MPa, respectively.
Liu
Lian
L
Electromechanics and Materials Engineering College, Dalian Maritime University, Dalian 116026, China. lliu@newmail.dlmu.edu.cn
Liu
Hui
H
Li
Xin
X
Zhang
Chunqing
C
D001840:Dental Bonding; D017220:Dentin-Bonding Agents / Q000138:chemical synthesis* / Q000737:chemistry; D006801:Humans; D008689:Methacrylates / Q000138:chemical synthesis* / Q000737:chemistry; D033081:Shear Strength
D017220:Dentin-Bonding Agents; D008689:Methacrylates; C069749:methacryloyloxydecyl dihydrogen phosphate