Synthesis and surface characterization of yttrium doped boehmite nanofibers.
Yttrium doped boehmite nanofibers with varying yttrium content have been synthesized at low temperatures using a soft-chemistry route in the presence of polyglycol ether surfactant. The effect of yttrium content, hydrothermal temperature on the growth of boehmite nanostructures was systematically studied. Nanofibers were formed in all samples with varying doped Y% treated at 100 degrees C; large Y(OH)(3) crystals were also formed at high yttrium doping. Treated at an elevated temperatures resulted in a remarkable changes in size and morphology for samples with the same doped Y content. The resultant nanofibers were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), selected area electron diffraction (SAED), energy-dispersive X-ray analysis (EDX), N(2) adsorption and thermogravimetric analysis. The detailed characterization and discussion on the Y doped nanostructures are presented.
Zhao
Yanyan
Y
Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, 2 George Street, GPO Box 2434, Brisbane, Queensland 4001, Australia.
Frost
Ray L
RL