90-kilobar diamond-anvil high-pressure cell for use on an automatic diffractometer.
A gasketed diamond-anvil high-pressure cell is described which can be used on a four-circle automatic diffractometer to collect x-ray intensity data from single-crystal samples subjected to truly hydrostatic pressures of over 90 kilobars. The force generating system exerts only forces normal to the diamond faces to obtain maximum reliability. A unique design allows exceptionally large open areas for maximum x-ray access and is particularly well suited for highly absorbing materials, as the x rays are not transmitted through the sample. Studies on ruby show that high-pressure crystal structure determinations may be done rapidly, reliably, and routinely with this system.
Schiferl
D
D
Department of Geophysical Sciences, University of Chicago, Chicago, IL 60637, USA.
Jamieson
J C
JC
Lenko
J E
JE