title: Multiple residue extraction for organochlorine pesticides in medicinal plants.
abstract: A rapid, multiresidue, multimatrix analytical method for the determination of aldrin, endrin, dieldrin and hexachlorocyclohexane isomers (alpha-, beta-, gamma- and delta-HCH) residues in medicinal plants has been developed. Samples were extracted by matrix solid-phase dispersion (MSPD) followed by gas chromatographic-electron-capture detection (GC-(63)Ni-ECD). The validation of the proposed approach was carried out by comparison with the European Pharmacopoeia reference extraction method obtaining similar or even better efficiencies by the proposed approach.
authors.affiliation: Eco-Auditing Group, National Botanical Research Institute, Council of Scientific and Industrial Research, Rana Pratap Marg, Lucknow, Uttar Pradesh, India. pcabhilash@gmail.com
authors.forename: P C
authors.initials: PC
authors.lastname: Abhilash
authors.forename: Nandita
authors.initials: N
authors.lastname: Singh
mesh_terms: D002849:Chromatography, Gas / Q000379:methods*; D006843:Hydrocarbons, Chlorinated / Q000032:analysis*; D010573:Pesticide Residues / Q000032:analysis; D010575:Pesticides / Q000032:analysis*; D010946:Plants, Medicinal / Q000737:chemistry*; D012989:Soil Pollutants / Q000032:analysis*
chemical_list: D006843:Hydrocarbons, Chlorinated; D010573:Pesticide Residues; D010575:Pesticides; D012989:Soil Pollutants