Confinement and step-wise reopening of channels in an artificial cell/inorganic capsule: a 7Li NMR study.
Haupt
Erhard T K
ETK
Department Chemie, Universität Hamburg, 20146 Hamburg (Germany), Fax: (+49) 40 428382893.
Wontorra
Claudia
C
Department Chemie, Universität Hamburg, 20146 Hamburg (Germany), Fax: (+49) 40 428382893.
Rehder
Dieter
D
Department Chemie, Universität Hamburg, 20146 Hamburg (Germany), Fax: (+49) 40 428382893.
Merca
Alice
A
Fakultät für Chemie der Universität, Postfach 100131, 33501 Bielefeld (Germany).
Müller
Achim
A
Fakultät für Chemie der Universität, Postfach 100131, 33501 Bielefeld (Germany).
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The 7Li-DOSY experiment was performed on a Bruker AVANCE-400 spectrometer by using a standard BBO-probehead with a Z-gradient. The ledbpgp2s-pulse-sequence[8] was applied. The T1 measurements were performed on a VARIAN-GEMINI-2000 spectrometer by using the standard VARIAN pulse sequence and T1 calculation software. The mean error was less than 0.2 s throughout all of the measurements.
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