Identification and characterization of solid-state nature of 2-chloromandelic acid.
The racemate and enantiomers of 2-chloromandelic acid were characterized by SS-NMR, XRPD, and FTIR. The binary melting point phase diagram was constructed by DSC (differential scanning calorimetry). The solid-state nature of 2-chloromandelic acid was identified to be a racemic compound. The crystal structure of racemic compound was determined to be monoclinic P2(1)/c.
Department of Chemical and Biochemical Engineering, the University of Western Ontario London, Ontario, Canada.
Quan
Q
He
Jesse
J
Zhu
Hassan
H
Gomaa
Michael
M
Jennings
Sohrab
S
Rohani
D002152:Calorimetry, Differential Scanning; D003460:Crystallization; D018360:Crystallography, X-Ray; D009682:Magnetic Resonance Spectroscopy; D008333:Mandelic Acids / Q000737:chemistry*; D008958:Models, Molecular; D008968:Molecular Conformation; D017550:Spectroscopy, Fourier Transform Infrared; D013237:Stereoisomerism; D014961:X-Ray Diffraction
C541344:2-chloromandelic acid; D008333:Mandelic Acids