Preparation of iodic acid by direct oxidation of iodine with perchloric acid dihydrate.
Iodine is quantitatively oxidised to iodic acid by boiling with 70% perchloric acid and the iodic acid is isolated by cooling, filtering off the precipitated crystals, and washing them with concentrated nitric acid. The over-all stoichiometry of the reaction is one molecule of perchloric acid per atom of iodine.
Hayes
J M
JM
Departments of Chemistry, Iowa State University, Ames, Iowa, and University of Illinois, Urbana, IllinoisU.S.A.
Diehl
H
H
Smith
G F
GF