Precipitation of bis(1,2-cyclohexanedionedioximato)palladium(II) from homogeneous solution.
The reaction between hydroxylamine and cyclohexanedione in the presence of palladium ions has been made the basis of the precipitation of bis(1,2-cyclohexanedionedioximato)palladium(II) from homogeneous solution. The procedure provides a means of separating palladium from Cu(II), Co(II), Ni(II) and Pt(IV), and is a simple, rapid and accurate method for determining palladium.
Velazquez
J A
JA
Burke Chemical Laboratories McMaster University Hamilton OntarioCanada.
Hileman
O E
OE