title: [Not Available].
abstract: The method for the determination of sulphur in organic compounds (E. Debal and R. Levy, Bull. Soc. Chim. France, 1968, 426; 1971, 3374) by combustion in oxygen at 1310-1320 degrees C and coulometric titration of the sulphur dioxide formed is improved. Silver and 8-hydroxy-quinoline are successfully used to remove halogens (fluorine included) from combustion products. A new glass cell for the acidimetric titration of sulphur dioxide with an automatic coulometer is devised, with a water-jacket for its cathodic and reference compartments. The constant-temperature water-flow makes this determination easy to carry out with no drawbacks, even in varying ambient temperature.
authors.affiliation: Service Central de Microanalyse du Centre National de la Recherche Scientifique 2 rue Henry Dunant-94320 Thiais, France.
authors.forename: D
authors.initials: D
authors.lastname: Fraisse
authors.forename: S
authors.initials: S
authors.lastname: Raveau