[Content comparison of diterpenoid pigments in different processed products of Gardenia jasminoides].
OBJECTIVE
To compare the contents of diterpenoid pigments in the different processed products of Gardenia jasminoides.


METHODS
The separation of Crocin 1, Crocin 2, Crocin 3, Crocetin were determined simultaneously by HPLC on a kromasil C18 column at 35 degrees C with the m methanol-acetonitrile-0.3% formic acid anhydrous in gradient elution as the mobile phrase. The detection wavelength was set at 440 nm and the flow rate was 1.0 mL x min(-1).


RESULTS
The obtained linearity of the four components was better over 0.9995 and the average recoveries were 97.77%, 100.05% , 98.40%, 101.02%, respectively.


CONCLUSIONS
The method is simple, accurate with good reproducibility. The results showed that the remarkable variation regulations appear among the different processed products.
Zhang
Cun
C
Institute of Chinese Materia Medica, China Academy of Chinese Medicial Sciences, Beijing 100700, China.
Xiao
Yong-Qing
YQ
Li
Li
L
Li
Gui-Liu
GL
Pang
Zhen
Z
D002338:Carotenoids / Q000737:chemistry; D002851:Chromatography, High Pressure Liquid; D004224:Diterpenes / Q000737:chemistry*; D004365:Drugs, Chinese Herbal / Q000737:chemistry*; D032062:Gardenia / Q000737:chemistry*; D015203:Reproducibility of Results; D014801:Vitamin A / Q000031:analogs & derivatives
D004224:Diterpenes; D004365:Drugs, Chinese Herbal; C487773:trans-sodium crocetinate; D014801:Vitamin A; D002338:Carotenoids; C029036:crocin