Analysis of polonium-210 in food products and bioassay samples by isotope-dilution alpha spectrometry.
A rapid and reliable radiochemical method coupled with a simple and compact plating apparatus was developed, validated, and applied for the analysis of (210)Po in variety of food products and bioassay samples. The method performance characteristics, including accuracy, precision, robustness, and specificity, were evaluated along with a detailed measurement uncertainty analysis. With high Po recovery, improved energy resolution, and effective removal of interfering elements by chromatographic extraction, the overall method accuracy was determined to be better than 5% with measurement precision of 10%, at 95% confidence level.
Lin
Zhichao
Z
Winchester Engineering and Analytical Center, Food and Drug Administration, 109 Holton Street, Winchester, MA 01890, USA. zhichao.lin@fda.hhs.gov
Wu
Zhongyu
Z
D000512:Alpha Particles; D002845:Chromatography; D005507:Food Contamination, Radioactive / Q000032:analysis*; D011059:Polonium / Q000032:analysis*; D013057:Spectrum Analysis / Q000379:methods
D011059:Polonium