Effects of adding methacrylate monomers on viscosity and mechanical properties of experimental light-curing soft lining materials based on urethane (meth)acrylate oligomers.
We investigated the viscosity and mechanical properties of experimental light-curing soft lining materials based on six commercially available urethane (meth)acrylate oligomers. The viscosities of the six oligomers were 1.9, 20.6, 26.8, 144.0, 185.3, and 8803.4 Pa*s at 25 degrees C. Two monomers (ethyl- and butyl-methacrylate) were added at 20 wt% to these oligomers to decrease the viscosity, resulting in viscosity reductions of 0.2 to 13.6 Pa*s for the six oligomers. The mechanical properties (compressive modulus, Shore A hardness, and tensile strength) were measured after two times light-polymerization for 3 min. The addition of the monomers to the oligomers only slightly changed the mechanical properties, in contrast to the large viscosity changes. Based on these results, it appears that the addition of ethyl- or butyl-methacrylate monomers is useful for decreasing the viscosity of experimental light-curing soft lining materials without changing their mechanical properties.
Kanie
Takahito
T
Department of Biomaterials Science, Graduate School of Medical and Dental Sciences, Kagoshima University, 8-35-1 Sakuragaoka, Kagoshima 890-8544, Japan. einak@ms.kagoshima-u.ac.jp
Kadokawa
Akihiko
A
Arikawa
Hiroyuki
H
Fujii
Koichi
K
Ban
Seiji
S
D000180:Acrylic Resins / Q000737:chemistry*; D019245:Compressive Strength; D003764:Dental Materials / Q000737:chemistry*; D003822:Denture Liners; D055119:Elastic Modulus; D006244:Hardness; D006801:Humans; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry*; D008768:Methylmethacrylates / Q000737:chemistry; D011140:Polyurethanes / Q000737:chemistry*; D013314:Stress, Mechanical; D013499:Surface Properties; D013997:Time Factors; D014783:Viscosity
D000180:Acrylic Resins; D003764:Dental Materials; D008689:Methacrylates; D008768:Methylmethacrylates; D011140:Polyurethanes; C050845:urethane acrylate; C009931:poly(ethylmethacrylate); C016284:butyl methacrylate