Preparation of 65Zn and 134Cs sealed sources based on commercial organic and synthesized inorganic sorbents for calibration purposes of gamma-detectors.
The sealed source of (65)Zn was prepared by using permutit as a commercial organic resin in an anion form, while in case of the (134)Cs, the sealed source was prepared by using the synthesized 12-molybdocerate(IV) gel as an inorganic exchanger in cation form. The batch technique was carried out for loading (65)Zn from 0.2 M HCl-60% acetone medium and for loading (134)Cs from 0.005 M HNO(3) onto the appropriate exchanger. The sealed source material of (65)Zn-permutit or (134)Cs-12-molybdocerate(IV), about 100 mg, was placed inside the cavity of a holder capsule (artelone) and its activity was measured to be 56.61+/-2.59 kBq (1.53+/-0.07 microCi) for (65)Zn on 21 April 2008 and 1.48+/-0.089 kBq (0.04+/-0.0024 microCi) for (134)Cs on 5 May 2008. The self absorption was calculated by using artelone and compared with the same thickness of stainless steel capsule as the holder material. The quality control was performed on the prepared sealed sources.
El-Azony
K M
KM
Radioactive Isotopes and Generators Department, Hot Lab Center, Atomic Energy Authority, PO Box 13759, Cairo, Egypt. mmenaa_2004@yahoo.com
El-Said
H
H
Mohty
A A
AA
D000327:Adsorption; D002138:Calibration; D002588:Cesium Radioisotopes; D005720:Gamma Rays; D015037:Zinc Radioisotopes
D002588:Cesium Radioisotopes; D015037:Zinc Radioisotopes