Isolation of chavibetol from essential oil of Pimenta pseudocaryophyllus leaf by high-speed counter-current chromatography.
Counter-current chromatography (CCC) was used to isolate chavibetol from the essential oil of leaves of Pimenta pseudocaryophyllus (Gomes) Landrum. Chavibetol was obtained in high purity (98%) and mass recovery (94.4%). Methyleugenol was also isolated. The CCC biphasic solvent system used was composed of hexane:n-butanol:methanol:water (12:4:4:3, v/v/v/v).
dos Santos
Bruna C B
BC
Universidade Estadual de Campinas, UNICAMP, Instituto de Química, SP, Brazil. brunacbsantos@yahoo.com
da Silva
Júlio César T
JC
Guerrero
Palimécio G
PG
Leitão
Gilda G
GG
Barata
Lauro E S
LE
D003377:Countercurrent Distribution / Q000379:methods*; D005054:Eugenol / Q000031:analogs & derivatives* / Q000737:chemistry / Q000302:isolation & purification; D009822:Oils, Volatile / Q000737:chemistry*; D027841:Pimenta / Q000737:chemistry*; D010936:Plant Extracts / Q000737:chemistry*; D018515:Plant Leaves / Q000737:chemistry*; D012997:Solvents / Q000737:chemistry
D009822:Oils, Volatile; D010936:Plant Extracts; D012997:Solvents; D005054:Eugenol; C542039:chavibetol