The influence of calcium chloride on the setting time, solubility, disintegration, and pH of mineral trioxide aggregate and white Portland cement with a radiopacifier.
This study evaluated the influence of addition of 10% calcium chloride (CaCl(2)) on the setting time, solubility, disintegration, and pH of white MTA (WMTA) and white Portland cement (WPC). A test of the setting time was performed following the #57 ADA specifications and a test of the final setting time according to the ASTM. For the solubility tests disintegration and pH, Teflon rings were filled with the cements and weighed after setting. After 24 h in a desiccator, they were once again weighed. Thereafter, they were immersed in MiliQ water for 24 and 72 h and 7, 14, and 28 days, with maintenance in the desiccator and weighing between periods. The pH of water in which the rings were immersed was measured immediately after contact with them and in the other periods. The addition of CaCl(2) provided a significant reduction (50%) in the initial setting time of cements. The final setting time of WMTA was reduced in 35.5% and the final setting time of WPC in 68.5%. The WMTA with CaCl(2) absorbed water and gained weight with time, except for in the 24-h period. The addition of CaCl(2) to the WPC reduced its solubility. The addition of CaCl(2) increased the pH of WMTA in the immediate period and at 24 and 72 h and for WPC in the immediate period and at 24 h. The addition of CaCl(2) to WMTA and WPC reduced the setting times and solubility of both and increased the pH of cements in the initial periods.
Bortoluzzi
Eduardo Antunes
EA
Dental School, Federal University of Santa Catarina, Florianópolis, Santa Catarina, Brazil. edubortoluzzi@hotmail.com
Broon
Norberto Juárez
NJ
Bramante
Clovis Monteiro
CM
Felippe
Wilson Tadeu
WT
Tanomaru Filho
Mario
M
Esberard
Roberto Miranda
RM
D017607:Aluminum Compounds / Q000138:chemical synthesis / Q000737:chemistry*; D002122:Calcium Chloride / Q000737:chemistry*; D017610:Calcium Compounds / Q000138:chemical synthesis / Q000737:chemistry*; D003287:Contrast Media; D003738:Dental Cements / Q000138:chemical synthesis / Q000737:chemistry; D004338:Drug Combinations; D006863:Hydrogen-Ion Concentration; D008422:Materials Testing; D010087:Oxides / Q000138:chemical synthesis / Q000737:chemistry*; D012387:Root Canal Filling Materials / Q000138:chemical synthesis / Q000737:chemistry*; D017640:Silicates / Q000138:chemical synthesis / Q000737:chemistry*; D012995:Solubility; D013997:Time Factors
D017607:Aluminum Compounds; D017610:Calcium Compounds; D003287:Contrast Media; D003738:Dental Cements; D004338:Drug Combinations; D010087:Oxides; D012387:Root Canal Filling Materials; D017640:Silicates; C472247:accelerated Portland cement; C086631:mineral trioxide aggregate; D002122:Calcium Chloride