title: Oxidative cyclization of alkenols with oxone using a miniflow reactor.
abstract: A miniflow system for oxidative cyclization of alkenols with Oxone was developed. Thus, the oxidative cyclization of (Z)- and (E)-alkenols in i-PrOH with an aqueous solution of Oxone proceeded smoothly and safely in a PTFE tube without any exogenous catalytic species, and was subsequently quenched in a flow-reaction manner to afford the corresponding furanyl and pyranyl carbinols quantitatively within 5 or 10 min of residence time.
authors.affiliation: RIKEN, Hirosawa, Wako, Saitama 351-0198, Japan.
authors.forename: Yoichi M A
authors.initials: YM
authors.lastname: Yamada
authors.forename: Kaoru
authors.initials: K
authors.lastname: Torii
authors.forename: Yasuhiro
authors.initials: Y
authors.lastname: Uozumi