title: A new small-angle X-ray scattering set-up on the crystallography beamline I711 at MAX-lab.
abstract: A small-angle X-ray scattering (SAXS) set-up has recently been developed at beamline I711 at the MAX II storage ring in Lund (Sweden). An overview of the required modifications is presented here together with a number of application examples. The accessible q range in a SAXS experiment is 0.009-0.3 A(-1) for the standard set-up but depends on the sample-to-detector distance, detector offset, beamstop size and wavelength. The SAXS camera has been designed to have a low background and has three collinear slit sets for collimating the incident beam. The standard beam size is about 0.37 mm x 0.37 mm (full width at half-maximum) at the sample position, with a flux of 4 x 10(10) photons s(-1) and lambda = 1.1 A. The vacuum is of the order of 0.05 mbar in the unbroken beam path from the first slits until the exit window in front of the detector. A large sample chamber with a number of lead-throughs allows different sample environments to be mounted. This station is used for measurements on weakly scattering proteins in solutions and also for colloids, polymers and other nanoscale structures. A special application supported by the beamline is the effort to establish a micro-fluidic sample environment for structural analysis of samples that are only available in limited quantities. Overall, this work demonstrates how a cost-effective SAXS station can be constructed on a multipurpose beamline.
authors.affiliation: MAX-lab, Lund University, POB 118, SE-22100 Lund, Sweden.
authors.forename: M
authors.initials: M
authors.lastname: Knaapila
authors.forename: C
authors.initials: C
authors.lastname: Svensson
authors.forename: J
authors.initials: J
authors.lastname: Barauskas
authors.forename: M
authors.initials: M
authors.lastname: Zackrisson
authors.forename: S S
authors.initials: SS
authors.lastname: Nielsen
authors.forename: K N
authors.initials: KN
authors.lastname: Toft
authors.forename: B
authors.initials: B
authors.lastname: Vestergaard
authors.forename: L
authors.initials: L
authors.lastname: Arleth
authors.forename: U
authors.initials: U
authors.lastname: Olsson
authors.forename: J S
authors.initials: JS
authors.lastname: Pedersen
authors.forename: Y
authors.initials: Y
authors.lastname: Cerenius
mesh_terms: D018360:Crystallography, X-Ray / Q000295:instrumentation*; D007768:Lactalbumin / Q000737:chemistry; D040901:Proteomics; D053838:Scattering, Small Angle
chemical_list: D007768:Lactalbumin