title: Corticosteroids 21-glucuronides: synthesis and complete characterization by (1)H and (13)C NMR.
abstract: Despite the important physiological role of the corticosteroids glucuronides, very poor NMR data for this class of compounds are reported. For this reason we prepared a set of corticosteroids and submitted them to a detailed NMR study. A complete assignment of (1)H and (13)C signals was accomplished arranging mono- and two-dimensional NMR techniques.
authors.affiliation: Dipartimento di Scienze Precliniche LITA Vialba, Università degli Studi di Milano, 20157 Milano, Italy.
authors.forename: Pierangela
authors.initials: P
authors.lastname: Ciuffreda
authors.forename: Silvana
authors.initials: S
authors.lastname: Casati
authors.forename: Maria
authors.initials: M
authors.lastname: De Mieri
authors.forename: Patrizia
authors.initials: P
authors.lastname: Ferraboschi
mesh_terms: D000305:Adrenal Cortex Hormones / Q000138:chemical synthesis* / Q000737:chemistry*; D020719:Glucuronides / Q000138:chemical synthesis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D013058:Mass Spectrometry
chemical_list: D000305:Adrenal Cortex Hormones; D020719:Glucuronides