Corticosteroids 21-glucuronides: synthesis and complete characterization by (1)H and (13)C NMR.
Despite the important physiological role of the corticosteroids glucuronides, very poor NMR data for this class of compounds are reported. For this reason we prepared a set of corticosteroids and submitted them to a detailed NMR study. A complete assignment of (1)H and (13)C signals was accomplished arranging mono- and two-dimensional NMR techniques.
Ciuffreda
Pierangela
P
Dipartimento di Scienze Precliniche LITA Vialba, Università degli Studi di Milano, 20157 Milano, Italy.
Casati
Silvana
S
De Mieri
Maria
M
Ferraboschi
Patrizia
P
D000305:Adrenal Cortex Hormones / Q000138:chemical synthesis* / Q000737:chemistry*; D020719:Glucuronides / Q000138:chemical synthesis* / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D013058:Mass Spectrometry
D000305:Adrenal Cortex Hormones; D020719:Glucuronides