Extraction with SPME and synthesis of 2-methyl-6-vinylpyrazine by a 'one pot' reaction using microwaves.
A synthesis of 2-methyl-6-vinylpyrazine was carried out by way of a 'one pot' reaction. In order to establish the efficiency of this synthesis the extraction of the volatiles released by male papaya fruit flies was performed by SPME (solid phase micro-extraction). The compound was separated and identified using GC/MSD (gas chromatography/mass spectrometry detector).
Robledo
Norma
N
Centro de Desarrollo de Productos Bióticos, IPN. Km. 8.5 Carretera Yautepec-Jojutla Yautepec, Morelos, C.P. 62731, Mexico.
Escalante
Jaime
J
Arzuffi
René
R
D000818:Animals; D001557:Benzenesulfonates / Q000737:chemistry*; D008401:Gas Chromatography-Mass Spectrometry; D009682:Magnetic Resonance Spectroscopy; D008297:Male; D008872:Microwaves; D015394:Molecular Structure; D011719:Pyrazines / Q000138:chemical synthesis* / Q000737:chemistry* / Q000302:isolation & purification; D033621:Tephritidae / Q000737:chemistry
D001557:Benzenesulfonates; D011719:Pyrazines; C056082:4-sulfophenylmethallyl ether