Determination of diacylhydrazines-type insect growth regulator JS-118 residues in cabbage and soil by high performance liquid chromatography with DAD detection.
JS-118 is a diacylhydrazines-type insect growth regulator used extensively in China now. An analytical method for residues determination of JS-118 in cabbage and soil samples by high performance liquid chromatography with DAD detection was established and optimized. Primary secondary amine solid phase extraction cartridge was used for sample preparation. Mean recoveries for the analyte ranged from 96.6% to 107.0% with CV value less than 4.7%. The limit of quantification is 0.01 mg/kg. Direct confirmation of JS-118 residues in samples was realized by high performance liquid chromatography-mass spectrometry. The proposed method is simple, rapid and reliable to perform and could be utilized for monitoring of pesticides residues.
Hu
J-Y
JY
School of Applied Science, University of Science and Technology Beijing, 100083 Beijing, China. jiyehu@sas.ustb.edu.cn
Deng
Z-B
ZB
Qin
D-M
DM
D001937:Brassica / Q000737:chemistry*; D002851:Chromatography, High Pressure Liquid; D005506:Food Contamination; D006834:Hydrazines / Q000032:analysis* / Q000737:chemistry; D007605:Juvenile Hormones / Q000032:analysis* / Q000737:chemistry; D010573:Pesticide Residues / Q000032:analysis* / Q000737:chemistry; D012987:Soil / Q000737:chemistry*
D006834:Hydrazines; C542015:JS-118; D007605:Juvenile Hormones; D010573:Pesticide Residues; D012987:Soil