Synthesis and spectral characterization of CoxMg1-xAl2O4 as new nano-coloring agent of ceramic pigment.
New nano-blue ceramic pigments of Co(x)Mg(1-x)Al(2)O(4) (0< or =x< or =0.1) have been prepared by co-precipitate-combustion as a hybrid method using urea as a fuel at 500 degrees C in open furnace in air atmosphere. The structure of pigment is assigned based on TGA/DTA/DrTGA analyses, X-ray diffraction (XRD) and transmission electron microscopy (TEM). Also, electronic spectra, infrared (IR) and diffuse reflectance spectroscopy (DRS) using CIE L*a*b* parameter measurement techniques were used. The results revealed that the nano-particle size of pigments were obtained in the range 30-38 nm as well as the varying colors and particle size as a result of different calcinations temperatures within the range of 500-1200 degrees C for 2h.
Ahmed
I S
IS
Chemistry Department, Faculty of Science, Benha University, Benha City, Egypt. isahmed61@gmail.com
Shama
S A
SA
Moustafa
M M
MM
Dessouki
H A
HA
Ali
A A
AA
D002516:Ceramics / Q000737:chemistry*; D004396:Coloring Agents / Q000737:chemistry*; D046529:Microscopy, Electron, Transmission; D010316:Particle Size; D013055:Spectrophotometry, Infrared; D014961:X-Ray Diffraction
D004396:Coloring Agents