Broadband carbon-13 correlation spectra of microcrystalline proteins in very high magnetic fields.
PARIS recoupling irradiation, despite a low rf amplitude, can promote efficient magnetization transfer during solid-state NMR experiments at 900 MHz over a wide range of differences in isotropic chemical shifts in microcrystalline proteins.
Weingarth
Markus
M
Département de Chimie, Ecole Normale Supérieure, 24 rue Lhomond, 75231 Paris cedex 05, France.
Bodenhausen
Geoffrey
G
Tekely
Piotr
P
D002247:Carbon Isotopes; D003460:Crystallization; D008280:Magnetics; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000379:methods*; D011506:Proteins / Q000737:chemistry*
D002247:Carbon Isotopes; D011506:Proteins