title: Heat treatment of a direct composite resin: influence on flexural strength.
abstract: The purpose of this study was to evaluate the flexural strength of a direct composite, for indirect application, that received heat treatment, with or without investment. One indirect composite was used for comparison. For determination of the heat treatment temperature, thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) were performed, considering the initial weight loss temperature and glass transition temperature (Tg). Then, after photoactivation (600 mW/cm(2) - 40 s), the specimens (10 x 2 x 2 mm) were heat-treated following these conditions: 170 masculineC for 5, 10 or 15 min, embedded or not embedded in investment. Flexural strength was assessed as a means to evaluate the influence of different heat treatment periods and investment embedding on mechanical properties. The data were analyzed by ANOVA and Tukey's test (alpha = 0.05). TGA showed an initial weight loss temperature of 180 masculineC and DSC showed a Tg value of 157 degrees C. Heat treatment was conducted in an oven (Flli Manfredi, Italy), after 37 degrees C storage for 48 h. Flexural strength was evaluated after 120 h at 37 degrees C storage. The results showed that different periods and investment embedding presented similar statistical values. Nevertheless, the direct composite resin with treatments presented higher values (178.7 MPa) compared to the indirect composite resin (146.0 MPa) and the same direct composite submitted to photoactivation only (151.7 MPa). Within the limitations of this study, it could be concluded that the heat treatment increased the flexural strength of the direct composite studied, leading to higher mechanical strength compared to the indirect composite.
authors.affiliation: Department of Biomaterials and Oral Biochemistry, University of São Paulo, SP, Brazil. clmiya@yahoo.com.br
authors.forename: Caroline Lumi
authors.initials: CL
authors.lastname: Miyazaki
authors.forename: Igor Studart
authors.initials: IS
authors.lastname: Medeiros
authors.forename: Ivone Lima
authors.initials: IL
authors.lastname: Santana
authors.forename: Jivaldo do Rosário
authors.initials: Jdo R
authors.lastname: Matos
authors.forename: Leonardo Eloy
authors.initials: LE
authors.lastname: Rodrigues Filho
mesh_terms: D002152:Calorimetry, Differential Scanning; D003188:Composite Resins / Q000737:chemistry*; D003799:Dental Stress Analysis; D006358:Hot Temperature; D008422:Materials Testing / Q000379:methods; D013718:Tensile Strength; D013818:Thermogravimetry
chemical_list: D003188:Composite Resins