title: Effect of argon purity on mechanical properties, microstructure and fracture mode of commercially pure (cp) Ti and Ti-6Al-4V alloys for ceramometal dental prostheses.
abstract: Provision of an inert gas atmosphere with high-purity argon gas is recommended for preventing titanium castings from contamination although the effects of the level of argon purity on the mechanical properties and the clinical performance of Ti castings have not yet been investigated. The purpose of this study was to evaluate the effect of argon purity on the mechanical properties and microstructure of commercially pure (cp) Ti and Ti-6Al-4V alloys. The castings were made using either high-purity and/or industrial argon gas. The ultimate tensile strength (UTS), proportional limit (PL), elongation (EL) and microhardness (VHN) at different depths were evaluated. The microstructure of the alloys was also revealed and the fracture mode was analyzed by scanning electron microscopy. The data from the mechanical tests and hardness were subjected to a two-and three-way ANOVA and Tukey's test (alpha = 0.05). The mean values of mechanical properties were not affected by the argon gas purity. Higher UTS, PL and VHN, and lower EL were observed for Ti-6Al-4V. The microhardness was not influenced by the argon gas purity. The industrial argon gas can be used to cast cp Ti and Ti-6Al-4V.
authors.affiliation: Department of Dentistry I, School of Dentistry, University Federal of Maranhão, Campus Universitário do Bacanga, Av. dos Portugueses, s/n, 65085680, São Luis/MA, Brazil. jrob@usp.br
authors.forename: José
authors.initials: J
authors.lastname: Bauer
authors.forename: Suelen
authors.initials: S
authors.lastname: Cella
authors.forename: Marcelo M
authors.initials: MM
authors.lastname: Pinto
authors.forename: Leonardo E Rodrigues
authors.initials: LE
authors.lastname: Filho
authors.forename: Alessandra
authors.initials: A
authors.lastname: Reis
authors.forename: Alessandro D
authors.initials: AD
authors.lastname: Loguercio
mesh_terms: D000497:Alloys; D001128:Argon / Q000737:chemistry*; D001672:Biocompatible Materials / Q000737:chemistry; D003722:Dental Alloys / Q000737:chemistry; D003735:Dental Casting Technique; D003764:Dental Materials / Q000737:chemistry; D017266:Dental Prosthesis; D005740:Gases; D006244:Hardness; D008422:Materials Testing; D008855:Microscopy, Electron, Scanning / Q000379:methods; D013314:Stress, Mechanical; D013718:Tensile Strength; D014025:Titanium / Q000737:chemistry*
chemical_list: D000497:Alloys; D001672:Biocompatible Materials; D003722:Dental Alloys; D003764:Dental Materials; D005740:Gases; C031462:titanium alloy (TiAl6V4); D001128:Argon; D014025:Titanium