Double-resonance magic angle coil spinning.
We present an extension of magic angle coil spinning (MACS) solid-state NMR spectroscopy to double-resonance experiments, enabling implementation of powerful double-resonance solid-state NMR methodologies including cross polarization, proton decoupling, and two-dimensional correlation spectroscopy etc., while still enjoying the merits that are intrinsic to MACS, such as high concentration sensitivity, eliminated magnetic susceptibility-induced field distortion, and an easy-to-use approach with the conventional and widespread hardware.
Inukai
Munehiro
M
Division of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo, 606-8502 Kyoto, Japan.
Takeda
Kazuyuki
K
D002247:Carbon Isotopes; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D009587:Nitrogen Isotopes; D011522:Protons; D012815:Signal Processing, Computer-Assisted; D012825:Silicon; D012975:Sodium Isotopes
D002247:Carbon Isotopes; D009587:Nitrogen Isotopes; D011522:Protons; D012975:Sodium Isotopes; D012825:Silicon