Efficient heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance at rotary resonance conditions.
We introduce here a heteronuclear dipolar decoupling scheme in solid-state nuclear magnetic resonance that performs efficiently at the rotary resonance conditions, where otherwise dipolar couplings are re-introduced. Results are shown proving the efficiency of this scheme at two magnetic fields under magic-angle spinning frequencies of 30 and 20 kHz.
Paul
Subhradip
S
Department of Chemical Sciences, Tata Institute of Fundamental Research, Homi Bhabha Road, Colaba, Mumbai 400 005, India.
Mithu
Venus Singh
VS
Kurur
Narayanan D
ND
Madhu
P K
PK
D000465:Algorithms; D003198:Computer Simulation; D003461:Crystallography; D004574:Electromagnetic Fields; D005998:Glycine / Q000737:chemistry; D019906:Nuclear Magnetic Resonance, Biomolecular / Q000295:instrumentation / Q000379:methods*
D005998:Glycine