title: Adhesive bond strengths to enamel and dentin using recommended and extended treatment times.
abstract: This study examined the effect of different enamel and dentin conditioning times on the shear bond strength of a resin composite using etch-and-rinse and self-etch adhesive systems. Shear bond strengths were determined following treatment of flat ground human enamel and dentin surfaces (4000 grit) with 11 adhesive systems: 1) AdheSE One Viva Pen-(ASE), 2) Adper Prompt L-Pop-(PLP), 3) Adper Single Bond Plus-(SBP), 4) Clearfil SE Bond-(CSE), 5) Clearfil S3 Bond-(CS3), 6) OptiBond All-In-One-(OBA), 7) OptiBond Solo Plus-(OBS), 8) Peak SE-(PSE), 9) Xeno IV-(X4), 10) Xeno V-(X5) and 11) XP Bond-(XPB) using recommended treatment times and an extended treatment time of 60 seconds (n = 10/group). Composite (Z100) to enamel and dentin bond strengths (24 hours) were determined using Ultradent fixtures and debonded with a crosshead speed of 1 mm/minute. The data were analyzed with a three-way Analysis of Variance (ANOVA) and Fisher's LSD post hoc test. The highest shear bond strengths (MPa) to enamel were achieved by the three etch-and-rinse systems at both the recommended treatment time (SBP-40.5 +/- 6.1; XPB-38.7 +/- 3.7; OBS- 35.2 +/- 6.2) and the extended treatment time (SBP-44.5 +/- 8.1; XPB-40.9 +/- 5.7; OBS-35.0 +/- 4.5). Extending the enamel treatment time did not produce a significant change (p > 0.05) in bond strength for the 11 adhesive systems tested. OBS generated the highest (46.2 +/- 7.9) bond strengths to dentin at the recommended treatment time. At the extended treatment time X4 (42.2 +/- 11.7), PSE (42.1 +/- 9.7) and OBS (41.4 +/- 8.0) produced the highest bond strengths to dentin. The bond strength change between recommend and extended treatment times was significant (p < 0.05) for PSE, but the other 10 systems did not exhibit any significant change.
authors.affiliation: Department of General Dentistry, Creighton University Medical Center, School of Dentistry, Omaha, Nebraska, USA. nsk@creighton.edu
authors.forename: Nicole S
authors.initials: NS
authors.lastname: Kimmes
authors.forename: Wayne W
authors.initials: WW
authors.lastname: Barkmeier
authors.forename: Robert L
authors.initials: RL
authors.lastname: Erickson
authors.forename: Mark A
authors.initials: MA
authors.lastname: Latta
mesh_terms: D000134:Acid Etching, Dental; D000180:Acrylic Resins / Q000737:chemistry; D017438:Bisphenol A-Glycidyl Methacrylate / Q000737:chemistry; D020770:Compomers / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003743:Dental Enamel / Q000648:ultrastructure*; D003799:Dental Stress Analysis / Q000295:instrumentation; D003804:Dentin / Q000648:ultrastructure*; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D006801:Humans; D008422:Materials Testing; D019279:Resin Cements / Q000737:chemistry; D033081:Shear Strength; D012822:Silicon Dioxide / Q000737:chemistry; D013314:Stress, Mechanical; D013997:Time Factors; D015040:Zirconium / Q000737:chemistry
chemical_list: D000180:Acrylic Resins; C489662:AdheSE cement; C505694:Clearfil S3 Bond; C438313:Clearfil SE Bond; D020770:Compomers; D003188:Composite Resins; D017220:Dentin-Bonding Agents; C451600:OptiBond Solo Plus; C092987:Optibond; C408584:Prompt L-Pop; D019279:Resin Cements; C511238:Single Bond Plus; C532387:XP-Bond; C417842:Xeno compomer; C083568:Z100 composite resin; D017438:Bisphenol A-Glycidyl Methacrylate; D012822:Silicon Dioxide; D015040:Zirconium