Natural abundance solid-state 95Mo MAS NMR of MoS2 reveals precise 95Mo anisotropic parameters from its central and satellite transitions.
Precise values are reported for a quite large (95)Mo quadrupole coupling and an unusually large (95)Mo chemical shift anisotropy in MoS(2), values that have been retrieved by analysis of a well-resolved, highly complex 14.1 T (95)Mo MAS NMR spectrum displaying both the central and satellite transitions.
Jakobsen
Hans J
HJ
Instrument Centre for Solid-State NMR Spectroscopy, Interdisciplinary Nanoscience Center (iNANO), Department of Chemistry, Aarhus University, DK-8000 Aarhus C, Denmark. hja@chem.au.dk
Bildsøe
Henrik
H
Skibsted
Jørgen
J
Brorson
Michael
M
Schaumburg
Kjeld
K