On the magic-angle turning and phase-adjusted spinning sidebands experiments.
The underlying relation between the magic-angle turning (MAT) and phase-adjusted spinning sidebands (PASS) experiments is examined. The MAT experiment satisfies the PASS conditions for separating spinning sidebands with a non-constant total evolution time and only requires linear t(1) increments of up to one rotor period. The time-domain data of the two experiments are related by a shearing transformation. A combination of the linear evolution-time increments of MAT and simple data processing of PASS are particularly attractive for the implementation of MAT for measuring chemical shift anisotropy.
Hung
Ivan
I
Center of Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 East Paul Dirac Drive, Tallahassee, FL 32310, USA.
Gan
Zhehong
Z
D000465:Algorithms; D016880:Anisotropy; D003198:Computer Simulation; D009682:Magnetic Resonance Spectroscopy / Q000379:methods*; D008956:Models, Chemical