Exploring the limits of (73)Ge solid-state NMR spectroscopy at ultrahigh magnetic field.
The ultrahigh field natural abundance (73)Ge solid-state wide-line NMR study of germanium dichloride complexed with 1,4-dioxane and tetraphenylgermane yields the largest (73)Ge quadrupolar coupling constant determined by NMR spectroscopy to date and the first direct observation of (73)Ge chemical shift anisotropy.
Sutrisno
Andre
A
Department of Chemistry, The University of Western Ontario, London, Ontario, CanadaN6A 5B7.
Hanson
Margaret A
MA
Rupar
Paul A
PA
Terskikh
Victor V
VV
Baines
Kim M
KM
Huang
Yining
Y