Sharp high-aspect-ratio AFM tips fabricated by a combination of deep reactive ion etching and focused ion beam techniques.
The shape and dimensions of an atomic force microscope tip are crucial factors to obtain high resolution images at the nanoscale. When measuring samples with narrow trenches, inclined sidewalls near 90 degrees or nanoscaled structures, standard silicon atomic force microscopy (AFM) tips do not provide satisfactory results. We have combined deep reactive ion etching (DRIE) and focused ion beam (FIB) lithography techniques in order to produce probes with sharp rocket-shaped silicon AFM tips for high resolution imaging. The cantilevers were shaped and the bulk micromachining was performed using the same DRIE equipment. To improve the tip aspect ratio we used FIB nanolithography technique. The tips were tested on narrow silicon trenches and over biological samples showing a better resolution when compared with standard AFM tips, which enables nanocharacterization and nanometrology of high-aspect-ratio structures and nanoscaled biological elements to be completed, and provides an alternative to commercial high aspect ratio AFM tips.
Caballero
David
D
Nanobioengineering group, Institute for Bioengineering of Catalonia, Barcelona Science Park, c/Baldiri Reixac 10-12, 08028 Barcelona, Spain
Villanueva
Guillermo
G
Plaza
Jose Antonio
JA
Mills
Christopher A
CA
Samitier
Josep
J
Errachid
Abdelhamid
A
D045744:Cell Line, Tumor; D006801:Humans; D018625:Microscopy, Atomic Force / Q000295:instrumentation* / Q000379:methods*; D008855:Microscopy, Electron, Scanning; D036103:Nanotechnology / Q000379:methods*; D010006:Osteoblasts / Q000648:ultrastructure; D019904:Polymethyl Methacrylate / Q000737:chemistry; D012825:Silicon / Q000737:chemistry
D019904:Polymethyl Methacrylate; D012825:Silicon