title: Producing samples for the organization of proficiency tests. Study of the homogeneity of replicas produced from two atmosphere generation systems.
abstract: This article describes two atmosphere generation systems used for the production of replicas. The first, the Sputnic system, is based on the Sputnic air sampler developed by the National Institute of Occupational Health in Oslo (Norway). It is used to generate asbestos fibres or silica particles and allows the simultaneous production, by means of sampling on filters, of up to 114 replicas. The second is a multipurpose system that allows dust sampling on foams used with the CIP 10-R device. Twenty samples can be taken simultaneously. In total, 120 series of samples allowed characterization of the variability of the two generation systems used for the production of replicas loaded with asbestos fibres or silica dust. The coefficients of variation characterizing the dispersion of the filter loading in the Sputnic system are <10% for high densities asbestos fibre or silica dust samples. The coefficient of dispersion is on average higher when the asbestos fibre density is lower. The differences observed between the measurements taken on the different crowns of the Sputnic system are low and <2%. The results obtained with the multipurpose system show that replica dispersion is on average equal to 4%, which will allow proposal in the near future of a proficiency test dedicated to the quantitative analysis of crystalline silica on foams sampled with the CIP 10-R device.
authors.affiliation: Institut national de recherche et de sécurité, Département métrologie des polluants, Vandoeuvre les Nancy, France. laurence.freville@inrs.fr
authors.forename: Laurence
authors.initials: L
authors.lastname: Freville
authors.forename: Jean-Claude
authors.initials: JC
authors.lastname: Moulut
authors.forename: Michel
authors.initials: M
authors.lastname: Grzebyk
authors.forename: Edmond
authors.initials: E
authors.lastname: Kauffer
mesh_terms: D000336:Aerosols; D000392:Air Movements; D000395:Air Pollutants, Occupational / Q000032:analysis* / Q000592:standards; D016902:Air Pollution, Indoor / Q000032:analysis / Q000706:statistics & numerical data; D000704:Analysis of Variance; D001194:Asbestos / Q000032:analysis; D001272:Atmosphere / Q000737:chemistry; D004391:Dust / Q000032:analysis; D004784:Environmental Monitoring / Q000295:instrumentation / Q000379:methods* / Q000592:standards; D004867:Equipment Design; D005374:Filtration / Q000295:instrumentation / Q000592:standards; D006801:Humans; D059021:Laboratory Proficiency Testing / Q000592:standards*; D019016:Mineral Fibers / Q000032:analysis / Q000706:statistics & numerical data; D016272:Occupational Health; D012015:Reference Standards; D012822:Silicon Dioxide / Q000032:analysis
chemical_list: D000336:Aerosols; D000395:Air Pollutants, Occupational; D004391:Dust; D019016:Mineral Fibers; D001194:Asbestos; D012822:Silicon Dioxide