[Condition optimization experiment of microwave extaction of flavonoids in rhizome of Drynaria fortunei].
The experiment extracted flavonoids in rhizome of Drynaria fortunei by microwave extraction, and determined the extraction rate through colorimetry. Through the single factor experiment and orthogonal method, the optimum extraction conditions were as follows: ethanol concentration was 40%, solid-liquid ratio was 1:20 (g/mL), microwave power was 325 W, extraction time was 40 s. Under these conditions, the extraction rate reached 1.73%. In all condtions, microwave power has the most significant effect on extraction rate. Microwave extraction has obvious advantages in comparison with traditional sovent refluxing method.
Yang
Bin
B
Jishou University/Key Laboratory of Plant Resources Conservation and Utilization of Hunan Province, Jishou 416000, China. thisyangbin@hotmail.com
Hu
Fu-chao
FC
Chen
Gong-xi
GX
Jiang
Dao-song
DS
D000431:Ethanol / Q000737:chemistry; D005419:Flavonoids / Q000032:analysis / Q000737:chemistry / Q000302:isolation & purification*; D008872:Microwaves; D018517:Plant Roots / Q000737:chemistry; D010946:Plants, Medicinal / Q000737:chemistry*; D029621:Polypodiaceae / Q000737:chemistry*; D027343:Rhizome / Q000737:chemistry; D012997:Solvents / Q000737:chemistry; D013678:Technology, Pharmaceutical / Q000379:methods; D013997:Time Factors
D005419:Flavonoids; D012997:Solvents; D000431:Ethanol