The effect of various mixing techniques on the surface microhardness of mineral trioxide aggregate.
OBJECTIVE
To evaluate the influence of various mixing procedures including ultrasonic vibration, trituration of customized encapsulated mineral trioxide aggregate (MTA) and condensation on the Vickers surface microhardness of MTA.


METHODS
ProRoot MTA Original, ProRoot MTA (white), MTA-Angelus (grey) and MTA White Angelus (white) were prepared using several mixing techniques including ultrasonic vibration, trituration of customized encapsulated MTA and conventional condensation. Twelve experimental groups (four materials: three techniques) were evaluated, each with 35 samples. All samples were incubated after preparation and subjected to Vickers surface microhardness testing after 4 and 28 days. Data was were subjected to a two-way anova.


RESULTS
At 28 days, the surface microhardness value was significantly greater for all experimental groups compared to 4 days after mixing (P < 0.00001). The application of ultrasonic energy to MTA produced significantly higher surface microhardness values compared to the other mixing techniques at both 4 and 28 days (P < 0.0001). However, no significant difference existed between condensation and trituration techniques at both time intervals. Regardless of the mixing technique employed, a significant difference (P < 0.0001) was observed in surface microhardness value between all types of MTA apart from between Angelus grey and ProRoot white at both 4 and 28 days, both of which produced the highest values.


CONCLUSIONS
Compared to trituration and condensation techniques, the application of ultrasonic energy to MTA produced a significantly higher surface microhardness value at both 4 and 28 days. Irrespective of mixing technique, ProRoot white and Angelus grey had the highest surface microhardness values. Trituration of encapsulated, premeasured MTA and water provides a standardiszed method of mixing that produces MTA slurries with more controllable handling characteristics.
Nekoofar
M H
MH
Department of Endodontics, Faculty of Dentistry, Tehran University of Medical Sciences, Tehran, Iran. nekoofar@yahoo.com
Aseeley
Z
Z
Dummer
P M H
PM
D017607:Aluminum Compounds / Q000138:chemical synthesis / Q000737:chemistry; D017610:Calcium Compounds / Q000138:chemical synthesis / Q000737:chemistry; D003799:Dental Stress Analysis; D004338:Drug Combinations; D004339:Drug Compounding / Q000379:methods*; D006244:Hardness; D008422:Materials Testing; D010087:Oxides / Q000138:chemical synthesis / Q000737:chemistry; D011312:Pressure; D012387:Root Canal Filling Materials / Q000138:chemical synthesis / Q000737:chemistry; D017640:Silicates / Q000138:chemical synthesis / Q000737:chemistry; D013499:Surface Properties; D014465:Ultrasonics; D014732:Vibration
D017607:Aluminum Compounds; D017610:Calcium Compounds; D004338:Drug Combinations; D010087:Oxides; D012387:Root Canal Filling Materials; D017640:Silicates; C086631:mineral trioxide aggregate