[Peculiarities of tetramethyltiuram disulfide detection in the biological material].
Optimal conditions for the extraction of tetramethyltiuram disulfide (TMTD) from biological materials with ethylacetate are described. The isolated compound can be separated from co-extracted impurities on a silicagel L (40/100 mcm) column. Identification and quantitative determination of TMTD purified from cadaverous liver were performed using thin-layer chromatography, IR spectrophotometry, and high performance liquid chromatography with UF detection.
Shormanov
V K
VK
Kim
A V
AV
Duritsyn
E P
EP
Baranov
Iu N
IuN
D000085:Acetates / Q000737:chemistry*; D000328:Adult; D002102:Cadaver; D002851:Chromatography, High Pressure Liquid / Q000379:methods; D002855:Chromatography, Thin Layer / Q000379:methods; D005554:Forensic Medicine / Q000379:methods*; D005659:Fungicides, Industrial / Q000032:analysis*; D006801:Humans; D008099:Liver / Q000737:chemistry*; D008297:Male; D012680:Sensitivity and Specificity; D013055:Spectrophotometry, Infrared / Q000379:methods; D013893:Thiram / Q000032:analysis*
D000085:Acetates; D005659:Fungicides, Industrial; D013893:Thiram; C007650:ethyl acetate