title: [Peculiarities of tetramethyltiuram disulfide detection in the biological material].
abstract: Optimal conditions for the extraction of tetramethyltiuram disulfide (TMTD) from biological materials with ethylacetate are described. The isolated compound can be separated from co-extracted impurities on a silicagel L (40/100 mcm) column. Identification and quantitative determination of TMTD purified from cadaverous liver were performed using thin-layer chromatography, IR spectrophotometry, and high performance liquid chromatography with UF detection.
authors.forename: V K
authors.initials: VK
authors.lastname: Shormanov
authors.forename: A V
authors.initials: AV
authors.lastname: Kim
authors.forename: E P
authors.initials: EP
authors.lastname: Duritsyn
authors.forename: Iu N
authors.initials: IuN
authors.lastname: Baranov
mesh_terms: D000085:Acetates / Q000737:chemistry*; D000328:Adult; D002102:Cadaver; D002851:Chromatography, High Pressure Liquid / Q000379:methods; D002855:Chromatography, Thin Layer / Q000379:methods; D005554:Forensic Medicine / Q000379:methods*; D005659:Fungicides, Industrial / Q000032:analysis*; D006801:Humans; D008099:Liver / Q000737:chemistry*; D008297:Male; D012680:Sensitivity and Specificity; D013055:Spectrophotometry, Infrared / Q000379:methods; D013893:Thiram / Q000032:analysis*
chemical_list: D000085:Acetates; D005659:Fungicides, Industrial; D013893:Thiram; C007650:ethyl acetate