Sonochemical synthesis and characterization of nano-belt lead(II) coordination polymer: new precursor to produce pure phase nano-sized lead(II) oxide.
Nanobelts of new a lead(II) coordination polymer, [Pb(3-pyc)(2)](n) (1), 3-Hpyc=3-pyridinecarboxilic acid were synthesized by a sonochemical method. The new nano-structure was characterized by scanning electron microscopy, X-ray powder diffraction, elemental analyses and IR spectroscopy. The thermal stability of compound was studied by thermal gravimetric and differential thermal analyses. After calcination of nano-sized compound 1 at 400°C, pure phase nano-sized lead(II) oxide has been produced.
Sadeghzadeh
Homa
H
Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14155-4838, Tehran, Iran.
Morsali
Ali
A
D007854:Lead / Q000737:chemistry*; D008422:Materials Testing; D008958:Models, Molecular; D049329:Nanostructures / Q000737:chemistry*; D036103:Nanotechnology; D009525:Niacin / Q000737:chemistry; D009942:Organometallic Compounds / Q000737:chemistry*; D010087:Oxides / Q000138:chemical synthesis* / Q000737:chemistry; D010316:Particle Size; D011108:Polymers / Q000737:chemistry*; D014465:Ultrasonics
D009942:Organometallic Compounds; D010087:Oxides; D011108:Polymers; D009525:Niacin; D007854:Lead; C047365:lead oxide