Rapid removal of selected volatile organic compounds from gaseous mixtures using a new dispersive vapor extraction technique: a feasibility study.
A new dispersive vapor extraction (DVE) technique for rapid removal of selected volatile organic compounds (VOCs) from gaseous mixtures was investigated. In this technique, less than 1.0 mL of a volatile solvent was vaporized for 8 min in a 250-mL flask containing a gaseous mixture. The flask was then cooled under running tap water for 2-3 min to induce condensation of the vapor and co-extraction of the VOCs from the headspace. The technique was tested over a concentration range of 4-23 ppb, and resulted in extraction efficiencies ranging from 80 to 97% for the VOCs tested. Because of its simplicity and the relatively short sampling time, DVE could potentially lead to high sample throughput and rapid air analysis.
Farrell
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Department of Health and Biomedical Sciences, Florida Hospital College of Health Sciences, Orlando, FL 32803, USA. sebastian.farrell@fhchs.edu
Pacey
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D002623:Chemistry Techniques, Analytical / Q000379:methods; D005240:Feasibility Studies; D005740:Gases / Q000737:chemistry*; D013997:Time Factors; D055549:Volatile Organic Compounds / Q000032:analysis* / Q000737:chemistry; D014835:Volatilization
D005740:Gases; D055549:Volatile Organic Compounds