Shear bond strength and ultrastructural interface analysis of different adhesive systems to bleached dentin.
BACKGROUND
It remains unclear as to whether or not dental bleaching affects the bond strength of dentin/resin restoration.


OBJECTIVE
To evaluated the bond strength of adhesive systems to dentin submitted to bleaching with 38% hydrogen peroxide (HP) activated by LED-laser and to assess the adhesive/dentin interfaces by means of SEM.


METHODS
Sixty fragments of dentin (25 mm²) were included and divided into two groups: bleached and unbleached. HP was applied for 20 s and photoactivated for 45 s. Groups were subdivided according to the adhesive systems (n = 10): (1) two-steps conventional system (Adper Single Bond), (2) two-steps self-etching system (Clearfil standard error (SE) Bond), and (3) one-step self-etching system (Prompt L-Pop). The specimens received the Z250 resin and, after 24 h, were submitted to the bond strength test. Additional 30 dentin fragments (n = 5) received the same surface treatments and were prepared for SEM. Data were analyzed by ANOVA and Tukey's test (α = 0.05).


RESULTS
There was significant strength reduction in bleached group when compared to unbleached group (P < 0.05). Higher bond strength was observed for Prompt. Single Bond and Clearfil presented the smallest values when used in bleached dentin. SEM analysis of the unbleached specimens revealed long tags and uniform hybrid layer for all adhesives. In bleached dentin, Single Bond provided open tubules and with few tags, Clearfil determined the absence of tags and hybrid layer, and Prompt promoted a regular hybrid layer with some tags.


CONCLUSIONS
Prompt promoted higher shear bond strength, regardless of the bleaching treatment and allowed the formation of a regular and fine hybrid layer with less deep tags, when compared to Single Bond and Clearfil.
Ferreira
Ernando A
EA
School of Dentistry, University of Ribeirão Preto, Ribeirão Preto, Brazil.
Souza-Gabriel
Aline E
AE
Silva-Sousa
Yara T C
YT
Sousa-Neto
Manoel D
MD
Silva
Ricardo G
RG
D000268:Adhesiveness / Q000187:drug effects; D003188:Composite Resins / Q000032:analysis / Q000737:chemistry*; D001840:Dental Bonding; D003738:Dental Cements / Q000737:chemistry*; D003793:Dental Restoration, Permanent; D003799:Dental Stress Analysis; D003804:Dentin / Q000737:chemistry* / Q000502:physiology / Q000648:ultrastructure; D006801:Humans; D006861:Hydrogen Peroxide / Q000737:chemistry / Q000494:pharmacology*; D008855:Microscopy, Electron, Scanning / Q000379:methods; D014070:Tooth / Q000187:drug effects; D014073:Tooth Bleaching / Q000009:adverse effects* / Q000379:methods
D003188:Composite Resins; D003738:Dental Cements; D006861:Hydrogen Peroxide