title: Dentin bond durability and water sorption/solubility of one-step self-etch adhesives.
abstract: The purpose of this study was to evaluate the dentin bonding durability of three HEMA-containing one-step self-etch adhesives after one-year water storage and to measure the amounts of their water sorption/solubility. OptiBond All-In-One (OP), Bond Force (BF) and Clearfil S³Bond (S³) were applied to the dentin surfaces according to manufacturers' instructions. Bond strengths to dentin were determined using µTBS test after water storage for 24 hours, six months, and one year. In addition, water sorption and solubility of the polymerized adhesives were measured. The µTBS of S³ and OP significantly decreased after one year. On the other hand, for BF there were no significant differences in µTBS between all storage periods. There were significant differences in water sorption and solubility among the adhesives (BF>S³>OP). The initial amounts of water sorption and solubility of the three adhesives did not affect their bonding durability to dentin.
authors.affiliation: Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University, 1-5-45 Yushima, Bunkyo-ku, Tokyo 113-8549, Japan. shima.itoh@gmail.com
authors.forename: Shima
authors.initials: S
authors.lastname: Itoh
authors.forename: Masatoshi
authors.initials: M
authors.lastname: Nakajima
authors.forename: Keiichi
authors.initials: K
authors.lastname: Hosaka
authors.forename: Masako
authors.initials: M
authors.lastname: Okuma
authors.forename: Masahiro
authors.initials: M
authors.lastname: Takahashi
authors.forename: Yuko
authors.initials: Y
authors.lastname: Shinoda
authors.forename: Naoko
authors.initials: N
authors.lastname: Seki
authors.forename: Masaomi
authors.initials: M
authors.lastname: Ikeda
authors.forename: Ryuzo
authors.initials: R
authors.lastname: Kishikawa
authors.forename: Richard M
authors.initials: RM
authors.lastname: Foxton
authors.forename: Junji
authors.initials: J
authors.lastname: Tagami
mesh_terms: D000042:Absorption; D000327:Adsorption; D017438:Bisphenol A-Glycidyl Methacrylate / Q000737:chemistry; D003188:Composite Resins / Q000737:chemistry; D001840:Dental Bonding; D003804:Dentin / Q000648:ultrastructure*; D017220:Dentin-Bonding Agents / Q000737:chemistry*; D006801:Humans; D008422:Materials Testing; D008689:Methacrylates / Q000737:chemistry; D008855:Microscopy, Electron, Scanning; D011092:Polyethylene Glycols / Q000737:chemistry; D058105:Polymerization; D011109:Polymethacrylic Acids / Q000737:chemistry; D019279:Resin Cements / Q000737:chemistry; D012995:Solubility; D013314:Stress, Mechanical; D013499:Surface Properties; D013718:Tensile Strength; D013997:Time Factors; D014867:Water / Q000737:chemistry*
chemical_list: C112828:Clearfil AP-X; C505694:Clearfil S3 Bond; D003188:Composite Resins; D017220:Dentin-Bonding Agents; D008689:Methacrylates; C092987:Optibond; D011109:Polymethacrylic Acids; D019279:Resin Cements; D014867:Water; C020946:triethylene glycol dimethacrylate; D011092:Polyethylene Glycols; D017438:Bisphenol A-Glycidyl Methacrylate; C005044:hydroxyethyl methacrylate