title: High-resolution solid-state (13)C μMAS NMR with long coherence life times.
abstract: Longer coherence life times (i.e. smaller homogeneous linewidths) can be achieved for carbon resonances which are strongly coupled to protons with high rf field heteronuclear decoupling in micro magic angle spinning NMR. Better proton decoupling enhances the sensitivity and resolution of two-dimensional through-bond correlation experiments for mass-limited samples with uniform carbon labeling.
authors.affiliation: Institute for Molecules and Materials, Radboud University Nijmegen, Heyendaalseweg 135, 6525 ED Nijmegen, The Netherlands. S.Vasa@nmr.ru.nl
authors.forename: Suresh K
authors.initials: SK
authors.lastname: Vasa
authors.forename: Hans
authors.initials: H
authors.lastname: Janssen
authors.forename: Ernst R H
authors.initials: ER
authors.lastname: Van Eck
authors.forename: Arno P M
authors.initials: AP
authors.lastname: Kentgens
mesh_terms: D002247:Carbon Isotopes; D005998:Glycine / Q000737:chemistry*; D009682:Magnetic Resonance Spectroscopy; D011522:Protons; D013997:Time Factors
chemical_list: D002247:Carbon Isotopes; D011522:Protons; D005998:Glycine