title: A convenient, high-sensitivity approach to multiple-resonance NMR at nanolitre volumes with inductively-coupled micro-coils.
abstract: We propose using singly-tuned μ-coils and (1)H-detection to obtain high-sensitivity in lieu of miniaturizing cumbersome multi-resonance circuits, with the existing MAS probe circuitry/coil providing RF at other frequencies. We demonstrate two key building blocks in solid-state NMR: cross-polarization and heteronuclear decoupling. As well, a (1)H-detected 2D HMQC is obtained.
authors.affiliation: CEA Saclay, IRAMIS, SIS2M, F-91191, Gif-sur-Yvette, France.
authors.forename: Pedro M
authors.initials: PM
authors.lastname: Aguiar
authors.forename: Jacques-François
authors.initials: JF
authors.lastname: Jacquinot
authors.forename: Dimitris
authors.initials: D
authors.lastname: Sakellariou